3-O,5-O-Dibenzyl-1-O,2-O-isopropylidene-6-deoxy-α-D-glucofuranose

Base Information

Chemical Name:3-O,5-O-Dibenzyl-1-O,2-O-isopropylidene-6-deoxy-α-D-glucofuranose
CAS No.:54522-22-4
Molecular Formula:
Molecular Weight:384.46542
Hs Code.:
Mol file:54522-22-4.mol

Synonyms:3-O,5-O-Dibenzyl-1-O,2-O-isopropylidene-6-deoxy-α-D-glucofuranose

Suppliers and Price of 3-O,5-O-Dibenzyl-1-O,2-O-isopropylidene-6-deoxy-α-D-glucofuranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 3-O,5-O-Dibenzyl-1-O,2-O-isopropylidene-6-deoxy-α-D-glucofuranose

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-O,5-O-Dibenzyl-1-O,2-O-isopropylidene-6-deoxy-α-D-glucofuranose

There total 10 articles about 3-O,5-O-Dibenzyl-1-O,2-O-isopropylidene-6-deoxy-α-D-glucofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 100-39-0
benzyl bromide

: 70632-45-0
(R)-1-((3aR,5R,6R,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)ethanol

: 54522-22-4
3,5-di-O-benzyl-1,2-O-isopropylidene-α-D-allofuranose

Guidance literature:: (R)-1-((3aR,5R,6R,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)ethanol; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

benzyl bromide; In N,N-dimethyl-formamide; at 18 ℃; for 4h; Cooling with ice;
DOI:10.1016/j.bioorg.2015.12.006

Reference yield: 74.0%

: 100-44-7
benzyl chloride

: 16749-46-5
6-deoxy-1,2-O-isopropylidene-β-L-idofuranose

: 28713-37-3,54522-22-4
3,5-di-O-benzyl-6-deoxy-1,2-O-isopropylidene-β-L-idofuranose

Guidance literature:: With potassium hydroxide; In N,N-dimethyl-formamide; at 23 - 27 ℃; for 1h;
DOI:10.1016/S0008-6215(00)81881-9

Reference yield: 60.0%

: 100-39-0
benzyl bromide

: 17668-66-5
6-deoxy-1,2-O-isopropylidene-α-D-glucofuranose

: 28713-29-3,54522-22-4
3,5-di-O-benzyl-6-deoxy-1,2-O-isopropylidene-α-D-glucofuranoside

Guidance literature:: 6-deoxy-1,2-O-isopropylidene-α-D-glucofuranose; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

benzyl bromide; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1002/ejoc.200801093