2,2'-Methylenedipiperidine

Base Information

Chemical Name:2,2'-Methylenedipiperidine
CAS No.:25382-41-6
Molecular Formula:C₁₁H₂₂N₂
Molecular Weight:182.309
Hs Code.:
Mol file:25382-41-6.mol

Synonyms:2,2'-Methylenedipiperidine

Suppliers and Price of 2,2'-Methylenedipiperidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2,2'-Methylenedipiperidine

Chemical Property:

Melting Point:54 - 55 °C
PSA：24.06000
LogP:2.31830

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,2'-Methylenedipiperidine

There total 9 articles about 2,2'-Methylenedipiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: bis(6-oxopiperidin-2-yl)methane

: 25382-41-6
bis(2-piperidinyl)methane

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 4h; Inert atmosphere; Reflux;
DOI:10.1002/ejoc.201801075

Reference yield: 66.0%

: 1132-37-2
bis(2-pyridyl)methane

: 25382-41-6
bis(2-piperidinyl)methane

Guidance literature:: With rhodium contaminated with carbon; hydrogen; acetic acid; In methanol; for 72h; under 63756.4 Torr; Autoclave;
DOI:10.1002/ejoc.201801075

Reference yield:

: 55100-61-3
2,2'-methylenedicyclopentanone

: 25382-41-6
bis(2-piperidinyl)methane

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid; sodium azide / chloroform / -15 °C / Reflux

2: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere; Reflux

With lithium aluminium tetrahydride; sodium azide; sulfuric acid; In tetrahydrofuran; chloroform; 1: |Schmidt Reaction;
DOI:10.1002/ejoc.201801075