2-Amino-2-oxo-acetic acid, N-[3,4-dimethylphenyl]-, ethyl ester

Base Information

• Chemical Name: 2-Amino-2-oxo-acetic acid, N-[3,4-dimethylphenyl]-, ethyl ester
• CAS No.: 24451-17-0
• Molecular Formula: C12H15NO3
• Molecular Weight: 221.256
• Hs Code.: 2924299090
• Mol file: 24451-17-0.mol

Synonyms:2-Amino-2-oxo-acetic acid, N-[3,4-dimethylphenyl]-, ethyl ester

Chemical Property of 2-Amino-2-oxo-acetic acid, N-[3,4-dimethylphenyl]-, ethyl ester

Chemical Property:

• PSA: 58.89000
• LogP: 2.45450

Purity/Quality:

98% ^*data from raw suppliers

Acetic acid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Amino-2-oxo-acetic acid, N-[3,4-dimethylphenyl]-, ethyl ester

There total 2 articles about 2-Amino-2-oxo-acetic acid, N-[3,4-dimethylphenyl]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Ethyl oxalyl chloride (4755-77-5) + 4-amino-o-xylene (95-64-7) → Ethyl[(3,4-dimethylphenyl)amino](oxo)acetate (24451-17-0)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 0.5h; Sealed tube;

DOI:10.1021/acscombsci.5b00091

Reference yield:

→ Ethyl[(3,4-dimethylphenyl)amino](oxo)acetate (24451-17-0)

Guidance literature:

Diethyloxalat, 3,4-Xylidin;

Reference yield:

ortho-methylbenzylamine (89-93-0) + Ethyl[(3,4-dimethylphenyl)amino](oxo)acetate (24451-17-0) → C18H20N2O2

Guidance literature:

In acetonitrile; at 100 ℃; for 6h;

DOI:10.1021/acscombsci.5b00091

upstream raw materials:

Ethyl oxalyl chloride

4-amino-o-xylene

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