Spermexatin

Base Information

Chemical Name:Spermexatin
CAS No.:117680-04-3
Molecular Formula:C₂₂H₄₀N₆O₉
Molecular Weight:532.594
Hs Code.:
DSSTox Substance ID:DTXSID00922516
Wikidata:Q82896072
Mol file:117680-04-3.mol

Synonyms:N(1),N(4),N(8)-tris(N-methyl-N-hydroxysuccinamoyl)spermidine;spermexatin

Suppliers and Price of Spermexatin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Spermexatin

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：231.67000
Density:1.278g/cm³
LogP:0.89910
XLogP3:-4.5
Hydrogen Bond Donor Count:7
Hydrogen Bond Acceptor Count:9
Rotatable Bond Count:20
Exact Mass:532.28567687
Heavy Atom Count:37
Complexity:750

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C(=O)CCC(=O)N(CCCCNC(=O)CCC(=O)NCO)CCCNC(=O)CCC(=O)NCO)O

Technology Process of Spermexatin

There total 8 articles about Spermexatin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 117680-01-0
N¹,N⁴,N⁸-Tris(N-methyl-N-(benzyloxy)succinamoyl)spermidine

: 117680-04-3
Spermexatin <2,2,2>

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 4h; Ambient temperature;
DOI:10.1021/jm00122a013

Reference yield:

: 117679-85-3
4-((benzyloxy)(methyl)amino)-4-oxobutanoic acid

: 117680-04-3
Spermexatin <2,2,2>

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / 1,3-dicyclohexylcarbodiimide / tetrahydrofuran / 1.) 0-5 deg C, 3 h, 2.) room temperature, 15 h

2: 52 percent / DMAP / tetrahydrofuran / 16 h / Ambient temperature

3: 83 percent / H₂ / 10percent Pd/C / ethanol / 4 h / Ambient temperature

With dmap; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1021/jm00122a013

Reference yield:

: 89965-56-0
<3-<<4-(carboxyamino)butyl>amino>propyl>carbamic acid, dibenzyl ester

: 117680-04-3
Spermexatin <2,2,2>

Guidance literature:: Multi-step reaction with 4 steps

1: DMAP / CH₂Cl₂ / 16 h

2: 1.) HBr/HOAc (33percent), 2.) NaHCO₃ / 1.) 4 h, room temperature, 2.) H₂O, ethyl acetate, 24 h, room temperature

3: 1.) N,N'-carbonyldiimidazole / 1.) CH₂Cl₂, 1 h, room temperature, 2.) CH₂Cl₂, 8 h

4: 83 percent / H₂ / 10percent Pd/C / ethanol / 4 h / Ambient temperature

With dmap; hydrogen bromide; hydrogen; sodium hydrogencarbonate; acetic acid; 1,1'-carbonyldiimidazole; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/jm00122a013