D-arabino-Hept-3-enitol, 1-amino-2,6-anhydro-1,3,4-trideoxy- (9CI)

Base Information

Chemical Name:D-arabino-Hept-3-enitol, 1-amino-2,6-anhydro-1,3,4-trideoxy- (9CI)
CAS No.:651302-70-4
Molecular Formula:C7H13NO3
Molecular Weight:159.18302
Hs Code.:
Mol file:651302-70-4.mol

Synonyms:D-arabino-Hept-3-enitol, 1-amino-2,6-anhydro-1,3,4-trideoxy- (9CI)

Suppliers and Price of D-arabino-Hept-3-enitol, 1-amino-2,6-anhydro-1,3,4-trideoxy- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of D-arabino-Hept-3-enitol, 1-amino-2,6-anhydro-1,3,4-trideoxy- (9CI)

Chemical Property:

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Technology Process of D-arabino-Hept-3-enitol, 1-amino-2,6-anhydro-1,3,4-trideoxy- (9CI)

There total 3 articles about D-arabino-Hept-3-enitol, 1-amino-2,6-anhydro-1,3,4-trideoxy- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 88180-36-3
2,3-dideoxy-α-D-erythro-hex-2-enopyranosyl cyanide

: 651302-70-4
1-aminomethyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranose

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 2.5h; Heating;
DOI:10.1081/CAR-120026469

Reference yield:

: 83938-00-5
((2R,3S,6S)-3-acetoxy-6-cyano-3,6-dihydro-2H-pyran-2-yl)methyl acetate

: 651302-70-4
1-aminomethyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / p-TsOH / methanol

2: 80 percent / LiAlH₄ / diethyl ether / 2.5 h / Heating

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; In methanol; diethyl ether;
DOI:10.1081/CAR-120026469

Reference yield:

: 2873-29-2
D-glucal triacetate

: 651302-70-4
1-aminomethyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: 38 percent / BF₃*Et₂O / CH₂Cl₂ / 0.08 h

2: 40 percent / p-TsOH / methanol

3: 80 percent / LiAlH₄ / diethyl ether / 2.5 h / Heating

With lithium aluminium tetrahydride; boron trifluoride diethyl etherate; toluene-4-sulfonic acid; In methanol; diethyl ether; dichloromethane;
DOI:10.1081/CAR-120026469