4,4-diethoxycyclohexanemethanol

Base Information

• Chemical Name: 4,4-diethoxycyclohexanemethanol
• CAS No.: 1232493-02-5
• Molecular Formula: C₁₁H₂₂O₃
• Molecular Weight: 202.294
• Mol file: 1232493-02-5.mol

Synonyms:4,4-diethoxycyclohexanemethanol

Chemical Property of 4,4-diethoxycyclohexanemethanol

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,4-diethoxycyclohexanemethanol

There total 1 articles about 4,4-diethoxycyclohexanemethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 4,4-diethoxycyclohexane-1carboxylate (860469-35-8) → (4,4-diethoxycyclohexyl)methanol (1232493-02-5)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 0.166667h;

Reference yield:

(4,4-diethoxycyclohexyl)methanol (1232493-02-5) + methyl iodide (74-88-4) → 1,1-diethoxy-4-(methoxymethyl)cyclohexane

Guidance literature:

(4,4-diethoxycyclohexyl)methanol; With sodium hydride; In tetrahydrofuran;

methyl iodide; In tetrahydrofuran;

Reference yield:

(4,4-diethoxycyclohexyl)methanol (1232493-02-5) → 4-(methoxymethyl)cyclohexan-1-one (17159-84-1)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran

2: acetic acid / water / 2 h / 65 °C

With sodium hydride; acetic acid; In tetrahydrofuran; water;

upstream raw materials:

ethyl 4,4-diethoxycyclohexane-1carboxylate

Downstream raw materials:

4-(methoxymethyl)cyclohexan-1-one