RARECHEM AX KI 1048

Base Information

Chemical Name:RARECHEM AX KI 1048
CAS No.:853680-02-1
Molecular Formula:C15H20ClNO4
Molecular Weight:313.781
Hs Code.:

Synonyms:RARECHEM AX KI 1048;4-CHLORO-A-[2-[[(1,1-DIMETHYLETHOXY)CARBONYL]AMINO]ETHYL]-BENZENEACETIC ACID

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Chemical Property of RARECHEM AX KI 1048

Chemical Property:

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Technology Process of RARECHEM AX KI 1048

There total 6 articles about RARECHEM AX KI 1048 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 853680-01-0
4-tert-butoxycarbonylamino-2-(4-chlorophenyl)-butyric acid ethyl ester

: 853680-02-1
4-tert-butoxycarbonylamino-2-(4-chlorophenyl)-butyric acid

Guidance literature:: 4-tert-butoxycarbonylamino-2-(4-chlorophenyl)-butyric acid ethyl ester; With lithium hydroxide; water; In tetrahydrofuran; at 0 - 20 ℃;

With hydrogenchloride; In tetrahydrofuran; water; pH=2 - 3;

Reference yield:

: 1878-66-6
4-chlorophenylacetic Acid

: 853680-02-1
4-tert-butoxycarbonylamino-2-(4-chlorophenyl)-butyric acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfuric acid / 20 °C

2.1: potassium tert-butylate / -78 - 20 °C

3.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C

4.1: diphenyl phosphoryl azide; triethylamine / dichloromethane / 3 h / 0 - 20 °C

5.1: tin(IV) chloride / dichloromethane / 1 h / 80 °C

6.1: lithium hydroxide; water / tetrahydrofuran / 0 - 20 °C

6.2: pH 2 - 3

With lithium hydroxide; diphenyl phosphoryl azide; potassium tert-butylate; water; tin(IV) chloride; triethylamine; trifluoroacetic acid; sulfuric acid; In tetrahydrofuran; dichloromethane;

Reference yield:

: 14062-24-9
4-chloro-benzeneacetic acid, ethyl ester

: 853680-02-1
4-tert-butoxycarbonylamino-2-(4-chlorophenyl)-butyric acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium tert-butylate / -78 - 20 °C

2.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C

3.1: diphenyl phosphoryl azide; triethylamine / dichloromethane / 3 h / 0 - 20 °C

4.1: tin(IV) chloride / dichloromethane / 1 h / 80 °C

5.1: lithium hydroxide; water / tetrahydrofuran / 0 - 20 °C

5.2: pH 2 - 3

With lithium hydroxide; diphenyl phosphoryl azide; potassium tert-butylate; water; tin(IV) chloride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;