Methyl 3-Boc-3-azabicyclo[3.1.1]heptane-6-carboxylate

Base Information

• Chemical Name: Methyl 3-Boc-3-azabicyclo[3.1.1]heptane-6-carboxylate
• CAS No.: 1363380-75-9
• Molecular Formula: C13H21NO4
• Molecular Weight: 255.31014
• Hs Code.: 2933998090
• Mol file: 1363380-75-9.mol

Synonyms:Methyl 3-Boc-3-azabicyclo[3.1.1]heptane-6-carboxylate;3-tert-Butyl 6-methyl 3-azabicyclo[3.1.1]heptane-3,6-dicarboxylate

Chemical Property of Methyl 3-Boc-3-azabicyclo[3.1.1]heptane-6-carboxylate

Chemical Property:

Purity/Quality:

99%, ^*data from raw suppliers

methyl3-boc-3-azabicyclo[3.1.1]heptane-6-carboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of Methyl 3-Boc-3-azabicyclo[3.1.1]heptane-6-carboxylate

There total 1 articles about Methyl 3-Boc-3-azabicyclo[3.1.1]heptane-6-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + methyl 3-azabicyclo[3.1.1]heptane-6-carboxylate hydrochloride (1389264-36-1) → 3-(tert-butyl) 6-methyl 3-azabicyclo[3.1.1]heptane-3,6-dicarboxylate (1363380-75-9)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 16h;

Reference yield:

3-(tert-butyl) 6-methyl 3-azabicyclo[3.1.1]heptane-3,6-dicarboxylate (1363380-75-9) → 3-(tert-butoxycarbonyl)-3-azabicyclo[3.1.1]heptane-6-carboxylic acid (1250995-41-5,1427460-12-5)

Guidance literature:

With water; lithium hydroxide; In tetrahydrofuran; at 20 ℃; for 5h;

upstream raw materials:

di-tert-butyl dicarbonate

methyl 3-azabicyclo[3.1.1]heptane-6-carboxylate hydrochloride

Downstream raw materials:

3-(tert-butoxycarbonyl)-3-azabicyclo[3.1.1]heptane-6-carboxylic acid

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