naphthalen-1-yl(1-tosyl-1H-pyrrol-3-yl)methanone

Base Information

• Chemical Name: naphthalen-1-yl(1-tosyl-1H-pyrrol-3-yl)methanone
• CAS No.: 129667-10-3
• Molecular Formula: C22H17NO3S
• Molecular Weight: 375
• Mol file: 129667-10-3.mol

Synonyms:naphthalen-1-yl(1-tosyl-1H-pyrrol-3-yl)methanone;1-Tosy-3-(1-naphthoyl)pyrrole;[1-[(4-Methylphenyl)sulfonyl]-1H-pyrrol-3-yl]-1-naphthalenyl-Methanone;1-[(4-Methylphenyl)sulfonyl]-3-(1-naphthalenylcarbonyl)-1H-pyrrole;1-Tosyl-3-(1-naphthoyl)pyrrole

Chemical Property of naphthalen-1-yl(1-tosyl-1H-pyrrol-3-yl)methanone

Chemical Property:

• PSA: 64.52000
• LogP: 5.49850

Purity/Quality:

97% ^*data from raw suppliers

Naphthalen-1-yl(1-tosyl-1H-pyrrol-3-yl)methanone 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 1-Tosyl-3-(1-naphthoyl)pyrrole can be used in the preparation of 1-alkyl-3-(1-naphthoyl)pyrroles, a new class of cannabinoid.

Technology Process of naphthalen-1-yl(1-tosyl-1H-pyrrol-3-yl)methanone

There total 2 articles about naphthalen-1-yl(1-tosyl-1H-pyrrol-3-yl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

N-p-toluenesulfonylpyrrole (17639-64-4) + naphthalene-1-carbonic acid chloride (879-18-5) → 2-(1-naphthoyl)-N-(p-toluenesulfonyl)pyrrole (129667-07-8) + 3-(1-naphthoyl)-N-(p-toluenesulfonyl)pyrrole (129667-10-3)

Guidance literature:

With aluminium trichloride;

Reference yield: 66.0%

N-p-toluenesulfonylpyrrole (17639-64-4) + naphthalene-1-carbonic acid chloride (879-18-5) → 3-(1-naphthoyl)-N-(p-toluenesulfonyl)pyrrole (129667-10-3)

Guidance literature:

With aluminium trichloride; In dichloromethane; at 0 - 20 ℃; for 2h;

DOI:10.1016/j.tet.2007.12.043

Reference yield: 96.0%

3-(1-naphthoyl)-N-(p-toluenesulfonyl)pyrrole (129667-10-3) → naphthalen-1-yl(1H-pyrrol-3-yl)methanone (162934-76-1)

Guidance literature:

With sodium hydroxide; In 1,4-dioxane; water; for 12h; Ambient temperature;

DOI:10.1016/0040-4039(95)00016-6

upstream raw materials:

N-p-toluenesulfonylpyrrole

naphthalene-1-carbonic acid chloride

Downstream raw materials:

3-[1,3]Dioxolan-2-yl-1-naphthalen-1-yl-1-[1-(toluene-4-sulfonyl)-1H-pyrrol-3-yl]-propan-1-ol

naphthalen-1-yl(1H-pyrrol-3-yl)methanone

4-(1-naphthyl)-1-tosylindole

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