2-Methoxymethyl-5-methyl-3-furancarboxylic acid methyl ester

Base Information

Chemical Name:2-Methoxymethyl-5-methyl-3-furancarboxylic acid methyl ester
CAS No.:35339-97-0
Molecular Formula:C₉H₁₂O₄
Molecular Weight:184.192
Hs Code.:
Mol file:35339-97-0.mol

Synonyms:2-Methoxymethyl-5-methyl-3-furancarboxylic acid methyl ester

Suppliers and Price of 2-Methoxymethyl-5-methyl-3-furancarboxylic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Methoxymethyl-5-methyl-3-furancarboxylic acid methyl ester

Chemical Property:

Boiling Point:249.9±40.0 °C(Predicted)
PSA：48.67000
Density:1.112±0.06 g/cm3(Predicted)
LogP:1.52100

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Methoxymethyl-5-methyl-3-furancarboxylic acid methyl ester

There total 3 articles about 2-Methoxymethyl-5-methyl-3-furancarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 2-(2-methoxyacetyl)methyl pent-4-enoate

: 35339-97-0
Methyl-5-methyl-2-methoxy-methyl-3-furoat

Guidance literature:: With dichloro bis(acetonitrile) palladium(II); oxygen; sodium acetate; lithium chloride; In N,N-dimethyl-formamide; at 40 ℃; for 24h; Molecular sieve;
DOI:10.1021/acs.joc.0c02777

Reference yield:

: 66762-68-3
ethyl 4-methoxy-3-oxobutanoate

: 35339-97-0
Methyl-5-methyl-2-methoxy-methyl-3-furoat

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 60 °C

2: sodium acetate; dichloro bis(acetonitrile) palladium(II); oxygen; lithium chloride / N,N-dimethyl-formamide / 24 h / 40 °C / Molecular sieve

With dichloro bis(acetonitrile) palladium(II); oxygen; sodium acetate; potassium carbonate; lithium chloride; In N,N-dimethyl-formamide; acetone;
DOI:10.1021/acs.joc.0c02777