tert-butyl 4-(3-oxo-3-phenylprop-1-enyl)piperidine-1-carboxylate

Base Information

Chemical Name:tert-butyl 4-(3-oxo-3-phenylprop-1-enyl)piperidine-1-carboxylate
CAS No.:291289-27-5
Molecular Formula:C₁₉H₂₅NO₃
Molecular Weight:315.412
Hs Code.:
Mol file:291289-27-5.mol

Synonyms:tert-butyl 4-(3-oxo-3-phenylprop-1-enyl)piperidine-1-carboxylate

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Chemical Property of tert-butyl 4-(3-oxo-3-phenylprop-1-enyl)piperidine-1-carboxylate

Chemical Property:

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Technology Process of tert-butyl 4-(3-oxo-3-phenylprop-1-enyl)piperidine-1-carboxylate

There total 5 articles about tert-butyl 4-(3-oxo-3-phenylprop-1-enyl)piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-(1-hydroxy-3-oxo-3-phenyl-propyl)-piperidine-1-carboxylic acid tert-butyl ester

: 291289-27-5
4-(3-oxo-3-phenyl-propenyl)-piperidine-1-carboxylic acid tert-butyl ester

Guidance literature:: With methanesulfonyl chloride; triethylamine; In dichloromethane;
DOI:10.1016/j.bmcl.2006.08.085

Reference yield:

: 6457-49-4
4-piperidinemethanol

: 291289-27-5
4-(3-oxo-3-phenyl-propenyl)-piperidine-1-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: CH₂Cl₂

2: DMSO; (COCl)2; Et₃N / CH₂Cl₂

3: LiHMDS / tetrahydrofuran

4: MeSO₂Cl; Et₃N / CH₂Cl₂

With oxalyl dichloride; dimethyl sulfoxide; methanesulfonyl chloride; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2006.08.085

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 291289-27-5
4-(3-oxo-3-phenyl-propenyl)-piperidine-1-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: CH₂Cl₂

2: DMSO; (COCl)2; Et₃N / CH₂Cl₂

3: LiHMDS / tetrahydrofuran

4: MeSO₂Cl; Et₃N / CH₂Cl₂

With oxalyl dichloride; dimethyl sulfoxide; methanesulfonyl chloride; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2006.08.085