3'-FLUORO-3-PHENYLPROPIOPHENONE

Base Information

• Chemical Name: 3'-FLUORO-3-PHENYLPROPIOPHENONE
• CAS No.: 898764-21-1
• Molecular Formula: C15H13FO
• Molecular Weight: 228.266
• Hs Code.: 2914700090
• Mol file: 898764-21-1.mol

Synonyms:3'-FLUORO-3-PHENYLPROPIOPHENONE

Chemical Property of 3'-FLUORO-3-PHENYLPROPIOPHENONE

Chemical Property:

• Vapor Pressure: 2.46E-05mmHg at 25°C
• Boiling Point: 358.9°C at 760 mmHg
• Flash Point: 150.2°C
• PSA: 17.07000
• Density: 1.127g/cm³
• LogP: 3.64120

Purity/Quality:

97% ^*data from raw suppliers

3'-fluoro-3-phenylpropiophenone 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3'-FLUORO-3-PHENYLPROPIOPHENONE

There total 10 articles about 3'-FLUORO-3-PHENYLPROPIOPHENONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

1-(3-fluorophenyl)ethanol (402-63-1) + benzyl alcohol (100-51-6,185532-71-2) → 1-(3-fluorophenyl)-3-phenylpropan-1-one (898764-21-1)

Guidance literature:

1-(3-fluorophenyl)ethanol; With Cp*Ir(6,6'-dionato-2,2'-bipyridine)(H₂O); In tert-Amyl alcohol; at 20 ℃; for 6h; Reflux;

benzyl alcohol; In tert-Amyl alcohol; for 6h; Reflux;

Reference yield: 79.0%

benzyl alcohol (100-51-6,185532-71-2) + 1-(3-fluorophenyl)ethanone (455-36-7) → 1-(3-fluorophenyl)-3-phenylpropan-1-one (898764-21-1)

Guidance literature:

With Cp*Ir(6,6'-dionato-2,2'-bipyridine)(H₂O); caesium carbonate; In tert-Amyl alcohol; for 6h; Reflux;

DOI:10.1021/acs.joc.5b01975

Reference yield: 72.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + 3-fluorobenzoic acid (455-38-9) → 1-(3-fluorophenyl)-3-phenylpropan-1-one (898764-21-1)

Guidance literature:

With 2,4,6-trimethyl-pyridine; methylene blue; triphenylphosphine; In N,N-dimethyl acetamide; at 20 ℃; Inert atmosphere; Irradiation;

upstream raw materials:

3-fluorophenylboronic acid

hydrocinnamic acid chloride

3-phenyl-propionaldehyde

3-chlorofluorobenzene

Downstream raw materials:

(E)-1-(3-fluorophenyl)-3-phenylprop-2-en-1-one

(S)-2-fluoro-1-(3-fluorophenyl)-2,3-diphenylpropan-1-one

2-bromo-2-fluoro-1-(3-fluorophenyl)-3-phenylpropan-1-one

C₁₅H₁₂F₂O

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