4,4,6-Trimethyl-2-(naphthalen-2-yl)-1,3,2-dioxaborinane

Base Information

• Chemical Name: 4,4,6-Trimethyl-2-(naphthalen-2-yl)-1,3,2-dioxaborinane
• CAS No.: 1260068-92-5
• Molecular Formula: C16H19BO2
• Molecular Weight: 254.137
• Hs Code.: 2931900090
• Mol file: 1260068-92-5.mol

Synonyms:4,4,6-Trimethyl-2-(naphthalen-2-yl)-1,3,2-dioxaborinane

Chemical Property of 4,4,6-Trimethyl-2-(naphthalen-2-yl)-1,3,2-dioxaborinane

Chemical Property:

• PSA: 18.46000
• LogP: 3.13900

Purity/Quality:

97% ^*data from raw suppliers

4,4,6-Trimethyl-2-(naphthalen-2-yl)-1,3,2-dioxaborinane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,4,6-Trimethyl-2-(naphthalen-2-yl)-1,3,2-dioxaborinane

There total 3 articles about 4,4,6-Trimethyl-2-(naphthalen-2-yl)-1,3,2-dioxaborinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2-bromonaphthalene (580-13-2) + 4,4,6-trimethyl-1,3,2-dioxaborinane (10199-14-1,23894-82-8) → 4,4,6-trimethyl-2-naphthalen-2-yl[1,3,2]dioxaborinane (1260068-92-5)

Guidance literature:

With 1,1'-bis-(diphenylphosphino)ferrocene; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); triethylamine; In toluene; at 100 ℃; for 18h;

DOI:10.3987/COM-12-S(N)28

Reference yield: 98.0%

2-methyl-2,4-pentanediol (107-41-5) + naphthalene-2-boronic acid (32316-92-0) → 4,4,6-trimethyl-2-naphthalen-2-yl[1,3,2]dioxaborinane (1260068-92-5)

Guidance literature:

In dichloromethane; at 20 ℃; for 16h;

DOI:10.1021/jacs.7b03387

Reference yield:

2-bromonaphthalene (580-13-2) + 4,4,6-trimethyl-1,3,2-dioxaborinane (10199-14-1,23894-82-8) → naphthalene (91-20-3,71998-51-1,72931-45-4) + 4,4,6-trimethyl-2-naphthalen-2-yl[1,3,2]dioxaborinane (1260068-92-5)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triethylamine; CyJohnPhos; In toluene; at 100 ℃; for 30h; Inert atmosphere;

DOI:10.1055/s-0030-1258059

upstream raw materials:

2-bromonaphthalene

4,4,6-trimethyl-1,3,2-dioxaborinane

2-methyl-2,4-pentanediol

naphthalene-2-boronic acid

Downstream raw materials:

2-benzylnaphthalene

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