6H-1,4-Dioxino[2,3-c]pyrrole-5,7-dicarboxylic acid, 6-ethyl-2,3-dihydro-

Base Information

Chemical Name:6H-1,4-Dioxino[2,3-c]pyrrole-5,7-dicarboxylic acid, 6-ethyl-2,3-dihydro-
CAS No.:943224-34-8
Molecular Formula:C₁₀H₁₁NO₆
Molecular Weight:241.2
Hs Code.:
Mol file:943224-34-8.mol

Synonyms:6H-1,4-Dioxino[2,3-c]pyrrole-5,7-dicarboxylic acid, 6-ethyl-2,3-dihydro-

Suppliers and Price of 6H-1,4-Dioxino[2,3-c]pyrrole-5,7-dicarboxylic acid, 6-ethyl-2,3-dihydro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6H-1,4-Dioxino[2,3-c]pyrrole-5,7-dicarboxylic acid, 6-ethyl-2,3-dihydro-

Chemical Property:

PSA：97.99000
LogP:0.67560

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6H-1,4-Dioxino[2,3-c]pyrrole-5,7-dicarboxylic acid, 6-ethyl-2,3-dihydro-

There total 3 articles about 6H-1,4-Dioxino[2,3-c]pyrrole-5,7-dicarboxylic acid, 6-ethyl-2,3-dihydro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 943224-33-7
diethyl N-ethyl-3,4-ethylenedioxypyrrole-2,5-dicarboxylate

: 943224-34-8
N-Ethyl-3,4-ethylenedioxypyrrole-2,5-dicarboxylic acid

: 1388133-20-7
2-ethyl N-ethyl-3,4-ethylenedioxypyrrole-2-carboxylate-5-carboxylic acid

Guidance literature:: With potassium tert-butylate; water; In tetrahydrofuran; at 0 - 20 ℃; for 16h;
DOI:10.1016/j.reactfunctpolym.2012.04.015

Reference yield:

: 35855-08-4
dimethyl N-ethyliminodiacetate

: 943224-34-8
N-Ethyl-3,4-ethylenedioxypyrrole-2,5-dicarboxylic acid

: 1388133-20-7
2-ethyl N-ethyl-3,4-ethylenedioxypyrrole-2-carboxylate-5-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: sodium ethanolate / 16 h / 78 °C

2: potassium carbonate / N,N-dimethyl-formamide / 16 h / 120 °C

3: potassium tert-butylate; water / tetrahydrofuran / 16 h / 0 - 20 °C

With potassium tert-butylate; water; sodium ethanolate; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.reactfunctpolym.2012.04.015

Reference yield:

: 100371-53-7
1-ethyl-3,4-dihydroxy-1H-pyrrole-2,5-dicarboxylic acid diethyl ester

: 943224-34-8
N-Ethyl-3,4-ethylenedioxypyrrole-2,5-dicarboxylic acid

: 1388133-20-7
2-ethyl N-ethyl-3,4-ethylenedioxypyrrole-2-carboxylate-5-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 120 °C

2: potassium tert-butylate; water / tetrahydrofuran / 16 h / 0 - 20 °C

With potassium tert-butylate; water; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.reactfunctpolym.2012.04.015