2-ethyl N-ethyl-3,4-ethylenedioxypyrrole-2-carboxylate-5-carboxylic acid

Base Information

Chemical Name:2-ethyl N-ethyl-3,4-ethylenedioxypyrrole-2-carboxylate-5-carboxylic acid
CAS No.:1388133-20-7
Molecular Formula:C₁₂H₁₅NO₆
Molecular Weight:269.254
Hs Code.:

Synonyms:2-ethyl N-ethyl-3,4-ethylenedioxypyrrole-2-carboxylate-5-carboxylic acid

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Chemical Property of 2-ethyl N-ethyl-3,4-ethylenedioxypyrrole-2-carboxylate-5-carboxylic acid

Chemical Property:

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Technology Process of 2-ethyl N-ethyl-3,4-ethylenedioxypyrrole-2-carboxylate-5-carboxylic acid

There total 4 articles about 2-ethyl N-ethyl-3,4-ethylenedioxypyrrole-2-carboxylate-5-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6096-81-7
dimethyl iminodiacetate

: 1388133-20-7
2-ethyl N-ethyl-3,4-ethylenedioxypyrrole-2-carboxylate-5-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 3 h / 100 °C

2: sodium ethanolate / 16 h / 78 °C

3: potassium carbonate / N,N-dimethyl-formamide / 16 h / 120 °C

4: potassium tert-butylate; water / tetrahydrofuran / 16 h / 0 - 20 °C

With potassium tert-butylate; water; sodium ethanolate; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.reactfunctpolym.2012.04.015

Reference yield:

: 943224-33-7
diethyl N-ethyl-3,4-ethylenedioxypyrrole-2,5-dicarboxylate

: 943224-34-8
N-Ethyl-3,4-ethylenedioxypyrrole-2,5-dicarboxylic acid

: 1388133-20-7
2-ethyl N-ethyl-3,4-ethylenedioxypyrrole-2-carboxylate-5-carboxylic acid

Guidance literature:: With potassium tert-butylate; water; In tetrahydrofuran; at 0 - 20 ℃; for 16h;
DOI:10.1016/j.reactfunctpolym.2012.04.015

Reference yield:

: 35855-08-4
dimethyl N-ethyliminodiacetate

: 943224-34-8
N-Ethyl-3,4-ethylenedioxypyrrole-2,5-dicarboxylic acid

: 1388133-20-7
2-ethyl N-ethyl-3,4-ethylenedioxypyrrole-2-carboxylate-5-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: sodium ethanolate / 16 h / 78 °C

2: potassium carbonate / N,N-dimethyl-formamide / 16 h / 120 °C

3: potassium tert-butylate; water / tetrahydrofuran / 16 h / 0 - 20 °C

With potassium tert-butylate; water; sodium ethanolate; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.reactfunctpolym.2012.04.015