[2-(4-Methylphenyl)phenyl]sulfonyl chloride

Base Information

Chemical Name:[2-(4-Methylphenyl)phenyl]sulfonyl chloride
CAS No.:173253-46-8
Molecular Formula:C13H11ClO2S
Molecular Weight:266.74324
Hs Code.:2904990090
DSSTox Substance ID:DTXSID40392037
Wikidata:Q82189936
Mol file:173253-46-8.mol

Synonyms:173253-46-8;[2-(4-METHYLPHENYL)PHENYL]SULFONYL CHLORIDE;2-(4-methylphenyl)benzenesulfonyl Chloride;4'-Methyl-[1,1'-biphenyl]-2-sulfonyl chloride;4'-Methyl-[1,1'-biphenyl]-2-sulphonyl chloride;SCHEMBL5682823;DTXSID40392037;RONQPPYFBKIXIJ-UHFFFAOYSA-N;AR1247;MFCD03840035;4'-methyl-2-biphenylsulphonyl chloride;4'-methyl biphenyl-2-sulfonyl chloride;AS-45067;CS-0172130;[2-(4-methylphenyl)phenyl]sulphonyl chloride;4'-Methyl-[1,1'-biphenyl]-2-sulfonylchloride;[2-(4-METHYLPHENYL)PHENYL]SULFONYLCHLORIDE;A907292;[2-(4-methylphenyl)phenyl]sulfonyl chloride, AldrichCPR

Suppliers and Price of [2-(4-Methylphenyl)phenyl]sulfonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynQuest Laboratories
4'-Methyl-[1,1'-biphenyl]-2-sulfonyl chloride
1 g
$ 1376.00

SynQuest Laboratories
4'-Methyl-[1,1'-biphenyl]-2-sulfonyl chloride
250 mg
$ 576.00

Crysdot
[2-(4-Methylphenyl)phenyl]sulfonylchloride 95+%
1g
$ 569.00

AK Scientific
[2-(4-Methylphenyl)phenyl]sulfonylchloride
1g
$ 851.00

AK Scientific
[2-(4-Methylphenyl)phenyl]sulfonylchloride
250mg
$ 385.00

Total 3 raw suppliers

Chemical Property of [2-(4-Methylphenyl)phenyl]sulfonyl chloride

Chemical Property:

PSA：42.52000
LogP:4.67030
XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:266.0168285
Heavy Atom Count:17
Complexity:339

Purity/Quality:

97% ^*data from raw suppliers

4'-Methyl-[1,1'-biphenyl]-2-sulfonyl chloride ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C2=CC=CC=C2S(=O)(=O)Cl

Technology Process of [2-(4-Methylphenyl)phenyl]sulfonyl chloride

There total 4 articles about [2-(4-Methylphenyl)phenyl]sulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5720-05-8
4-methylphenylboronic acid

: 173253-46-8
4'-methyl-2-biphenylsulphonyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: 97 percent / aq. Na₂CO₃ / (Ph₃P)4Pd / 1,2-dimethoxy-ethane / 12 h / 100 °C

2.1: H₂ / Raney Ni / methanol; tetrahydrofuran / 6 h / 2585.74 Torr

3.1: NaNO₂; conc. HCl / acetic acid; H₂O / -5 - 0 °C

3.2: SO₂; CuCl / acetic acid; H₂O / 12 h / 50 °C

With hydrogenchloride; hydrogen; sodium carbonate; sodium nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; nickel; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; water; acetic acid;
DOI:10.1016/S0968-0896(01)00250-4

Reference yield:

: 1204-43-9
2-(4-methylphenyl)aniline

: 173253-46-8
4'-methyl-2-biphenylsulphonyl chloride

Guidance literature:: 2-(4-methylphenyl)aniline; With hydrogenchloride; sodium nitrite; In water; acetic acid; at -5 - 0 ℃;

With sulfur dioxide; copper(l) chloride; In water; acetic acid; at 50 ℃; for 12h;
DOI:10.1016/S0968-0896(01)00250-4

Reference yield:

: 70680-21-6
4-methyl-2'-nitrobiphenyl

: 173253-46-8
4'-methyl-2-biphenylsulphonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: H₂ / Raney Ni / methanol; tetrahydrofuran / 6 h / 2585.74 Torr

2.1: NaNO₂; conc. HCl / acetic acid; H₂O / -5 - 0 °C

2.2: SO₂; CuCl / acetic acid; H₂O / 12 h / 50 °C

With hydrogenchloride; hydrogen; sodium nitrite; nickel; In tetrahydrofuran; methanol; water; acetic acid;
DOI:10.1016/S0968-0896(01)00250-4