Trans-2-fluorocyclopropanamine hydrochloride

Base Information

• Chemical Name: Trans-2-fluorocyclopropanamine hydrochloride
• CAS No.: 114152-96-4
• Molecular Formula: C₃H₆FN*ClH
• Molecular Weight: 111.547
• Hs Code.: 2921309990
• Mol file: 114152-96-4.mol

Synonyms:Trans-2-fluorocyclopropanamine hydrochloride

Chemical Property of Trans-2-fluorocyclopropanamine hydrochloride

Chemical Property:

• PSA: 0.00000
• LogP: 0.00000
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

trans-2-Fluorocyclopropanaminehydrochloride 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of Trans-2-fluorocyclopropanamine hydrochloride

There total 10 articles about Trans-2-fluorocyclopropanamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

benzyl N-benzyl-N-<(1R*,2S*)-2-fluorocyclopropyl>carbamate (142977-37-5,142977-43-3,146657-23-0,146657-24-1) → (1R*,2S*)-2-fluorocyclopropylamine hydrochloride (114152-95-3,114152-96-4,141042-20-8,141042-21-9,143062-71-9,143062-74-2,143062-85-5)

Guidance literature:

With hydrogen; palladium on activated charcoal; under 2206.5 - 2942.03 Torr; Ambient temperature; 1.) AcOH, 2.) HCl/MeOH;

DOI:10.1016/S0040-4039(00)92669-8

Reference yield: 83.0%

benzyl N-benzyl-N-<(1R*,2R*)-2-fluorocyclopropyl>carbamate (142977-37-5,142977-43-3,146657-23-0,146657-24-1) → (1R*,2R*)-2-fluorocyclopropylamine hydrochloride (114152-95-3,114152-96-4,141042-20-8,141042-21-9,143062-71-9,143062-74-2,143062-85-5)

Guidance literature:

With hydrogen; palladium on activated charcoal; In acetic acid; under 2206.5 - 2942.03 Torr; Ambient temperature;

DOI:10.1016/S0040-4039(00)92669-8

Reference yield: 77.0%

benzyl N-<(1R*,2S*)-2-fluorocyclopropyl>-N-(1-phenylethyl)carbamate (142977-39-7,151123-40-9,151123-41-0,151123-42-1,151123-43-2) → (1R*,2S*)-2-fluorocyclopropylamine hydrochloride (114152-95-3,114152-96-4,141042-20-8,141042-21-9,143062-71-9,143062-74-2,143062-85-5)

Guidance literature:

With hydrogen; palladium on activated charcoal; under 2206.5 - 2942.03 Torr; Ambient temperature; 1.) AcOH, 2.) HCl/MeOH;

DOI:10.1016/S0040-4039(00)92669-8

upstream raw materials:

benzyl N-benzyl-N-<(1R*,2R*)-2-fluorocyclopropyl>carbamate

t-butyl N-benzyl-N-<(1R*,2S*)-2-fluorocyclopropyl>carbamate

benzyl N-benzyl-N-<(1R*,2S*)-2-fluorocyclopropyl>carbamate

t-butyl N-<(1R*,2S*)-2-fluorocyclopropyl>-N-(1-phenylethyl)carbamate

Downstream raw materials:

tert-butyl dl-N-(trans-2-fluorocyclopropyl)carbamate

tert-butyl dl-N-(cis-2-fluorocyclopropyl)carbamate

(-)-cis-2-fluorocyclopropylamine hydrochloride

(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl N-(1R,2S)-2-fluorocyclopropylcarbamate

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