(6aR-trans)-1-[(tert-Butyl)diMethylsilyloxy]-6a,7,8,1

Base Information

• Chemical Name: (6aR-trans)-1-[(tert-Butyl)diMethylsilyloxy]-6a,7,8,1
• CAS No.: 124588-22-3
• Molecular Formula: C27H44O3Si
• Molecular Weight: 444.73
• Mol file: 124588-22-3.mol

Synonyms:(6aR-trans)-1-[(tert-Butyl)diMethylsilyloxy]-6a,7,8,1;1-O-[(tert-Butyl)diMethylsilyloxy]-11-hydroxy-9-tetrahydro Cannabinol

Chemical Property of (6aR-trans)-1-[(tert-Butyl)diMethylsilyloxy]-6a,7,8,1

Chemical Property:

• PSA: 38.69000
• LogP: 7.38660

Purity/Quality:

1-O-[(tert-Butyl)dimethylsilyloxy]-11-hydroxy-delta9-tetrahydro cannabinol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: (6aR-trans)-1-[(tert-Butyl)diMethylsilyloxy]-6a,7,8,1 is used in the preparation of Tetrahydrocannabinol (T293200) derivatives.

Technology Process of (6aR-trans)-1-[(tert-Butyl)diMethylsilyloxy]-6a,7,8,1

There total 1 articles about (6aR-trans)-1-[(tert-Butyl)diMethylsilyloxy]-6a,7,8,1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Acetic acid (6aR,10aR)-1-(tert-butyl-dimethyl-silanyloxy)-6,6-dimethyl-3-pentyl-6a,7,8,10a-tetrahydro-6H-benzo[c]chromen-9-ylmethyl ester → [(6aR,10aR)-1-(tert-Butyl-dimethyl-silanyloxy)-6,6-dimethyl-3-pentyl-6a,7,8,10a-tetrahydro-6H-benzo[c]chromen-9-yl]-methanol (124588-22-3)

Guidance literature:

With lithium aluminium tetrahydride;

DOI:10.1039/c39890000062

Reference yield:

[(6aR,10aR)-1-(tert-Butyl-dimethyl-silanyloxy)-6,6-dimethyl-3-pentyl-6a,7,8,10a-tetrahydro-6H-benzo[c]chromen-9-yl]-methanol (124588-22-3) → 11-nor-9-carboxt-Δ-9-tetrahydrocannabinol (36557-05-8,56354-06-4,64280-14-4,104874-50-2,114028-39-6,122797-75-5)

Guidance literature:

Multi-step reaction with 2 steps

1: Swern reagent

2: sodium chlorite, 2-methylbut-2-ene

With sodium chlorite; swern reagent; 2-methyl-but-2-ene;

DOI:10.1039/c39890000062

Reference yield:

[(6aR,10aR)-1-(tert-Butyl-dimethyl-silanyloxy)-6,6-dimethyl-3-pentyl-6a,7,8,10a-tetrahydro-6H-benzo[c]chromen-9-yl]-methanol (124588-22-3) → (-)-11-nor-9-carboxy-Δ9-tetrahydrocannabinol tert-butyldimethylsilyl ether (138285-38-8)

Guidance literature:

With swern reagent;

DOI:10.1039/c39890000062

Downstream raw materials:

(-)-11-nor-9-carboxy-Δ⁹-tetrahydrocannabinol tert-butyldimethylsilyl ether

11-nor-9-carboxt-Δ-9-tetrahydrocannabinol

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