ethyl 2-aMino-1-(5-chlorobenzo[b]thiophen-3-yl)-2-oxoethyl(Methyl)phosphinate

Base Information

• Chemical Name: ethyl 2-aMino-1-(5-chlorobenzo[b]thiophen-3-yl)-2-oxoethyl(Methyl)phosphinate
• CAS No.: 1206680-28-5
• Molecular Formula: C13H15ClNO3PS
• Molecular Weight: 331.754861
• Hs Code.: 2934999090
• Mol file: 1206680-28-5.mol

Synonyms:ethyl 2-aMino-1-(5-chlorobenzo[b]thiophen-3-yl)-2-oxoethyl(Methyl)phosphinate;[Carbamoyl-(5-chloro-benzo[b]thiophen-3-yl)-methyl]methyl phosphinic acid ethyl ester

Chemical Property of ethyl 2-aMino-1-(5-chlorobenzo[b]thiophen-3-yl)-2-oxoethyl(Methyl)phosphinate

Chemical Property:

• PSA: 107.44000
• LogP: 4.72580

Purity/Quality:

99%, ^*data from raw suppliers

Ethyl (2-amino-1-(5-chlorobenzo[b]thiophen-3-yl)-2-oxoethyl)(methyl)phosphinate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ethyl 2-aMino-1-(5-chlorobenzo[b]thiophen-3-yl)-2-oxoethyl(Methyl)phosphinate

There total 2 articles about ethyl 2-aMino-1-(5-chlorobenzo[b]thiophen-3-yl)-2-oxoethyl(Methyl)phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C16H16ClN2O3PS → [carbamoyl(5-chlorobenzo[b]thiophen-3-yl)methyl]-methylphosphinic acid ethyl ester (1206680-28-5)

Guidance literature:

With ammonia; In N,N-dimethyl-formamide; at 0 ℃;

Reference yield:

C18H22ClO5PS → [carbamoyl(5-chlorobenzo[b]thiophen-3-yl)methyl]-methylphosphinic acid ethyl ester (1206680-28-5)

Guidance literature:

With ammonium acetate; In tetrahydrofuran; at -2 ℃;

Reference yield:

4-(2-bromovinyl)-1,2-difluorobenzene (1206708-55-5) + [carbamoyl(5-chlorobenzo[b]thiophen-3-yl)methyl]-methylphosphinic acid ethyl ester (1206680-28-5) → {(5-chlorobenzo[b]thiophen-3-yl)[2-(3,4-difluorophenyl)vinylcarbamoyl]methyl}-methylphosphinic acid ethyl ester (936366-46-0)

Guidance literature:

[carbamoyl(5-chlorobenzo[b]thiophen-3-yl)methyl]-methylphosphinic acid ethyl ester; With caesium carbonate; N,N`-dimethylethylenediamine; copper(l) iodide; In N,N-dimethyl acetamide; at 20 - 75 ℃; Inert atmosphere;

4-(2-bromovinyl)-1,2-difluorobenzene; In N,N-dimethyl acetamide; at 75 - 85 ℃; Product distribution / selectivity; Inert atmosphere;

Downstream raw materials:

{(5-chlorobenzo[b]thiophen-3-yl)[2-(3,4-difluorophenyl)vinylcarbamoyl]methyl}-methylphosphinic acid ethyl ester

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