3,6-Dichloro-4-iodopyridazine

Base Information

• Chemical Name: 3,6-Dichloro-4-iodopyridazine
• CAS No.: 130825-13-7
• Molecular Formula: C4HCl2IN2
• Molecular Weight: 274.87
• Hs Code.: 2933998090
• Mol file: 130825-13-7.mol

Synonyms:3,6-Dichloro-4-iodopyridazine

Chemical Property of 3,6-Dichloro-4-iodopyridazine

Chemical Property:

• PSA: 25.78000
• LogP: 2.38800
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

97% ^*data from raw suppliers

3,6-Dichloro-4-iodopyridazine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,6-Dichloro-4-iodopyridazine

There total 3 articles about 3,6-Dichloro-4-iodopyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

(3,6-dichloropyridazin-4-yl)zinc pivalate → 3,6-Dichloro-4-iodopyridazine (130825-13-7)

Guidance literature:

With iodine; In tetrahydrofuran; at 25 ℃; for 1h; Inert atmosphere;

DOI:10.1002/chem.201403015

Reference yield: 84.0%

3,6-dichlorpyridazine (141-30-0) → 3,6-Dichloro-4-iodopyridazine (130825-13-7)

Guidance literature:

3,6-dichlorpyridazine; With zinc chloride-2,2,6,6-tetramethylpiperidin-1-ide lithium chloride complex; In tetrahydrofuran; at 25 ℃; for 0.5h; Inert atmosphere;

With iodine; In tetrahydrofuran; for 0.5h; Inert atmosphere;

DOI:10.1021/ol900342a

Reference yield: 82.0%

C8H2Cl4N4Zn (1104202-03-0) → 3,6-Dichloro-4-iodopyridazine (130825-13-7)

Guidance literature:

With iodine; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

DOI:10.1039/b815903c

upstream raw materials:

3,6-dichlorpyridazine

C₈H₂Cl₄N₄Zn