tert-butyl 2-(3-chlorophenyl)-2-hydroxyethylcarbamate

Base Information

Chemical Name:tert-butyl 2-(3-chlorophenyl)-2-hydroxyethylcarbamate
CAS No.:1187983-89-6
Molecular Formula:C₁₃H₁₈ClNO₃
Molecular Weight:271.744
Hs Code.:
Mol file:1187983-89-6.mol

Synonyms:tert-butyl 2-(3-chlorophenyl)-2-hydroxyethylcarbamate;2-(Boc-amino)-1-(3-chlorophenyl)ethanol

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Chemical Property of tert-butyl 2-(3-chlorophenyl)-2-hydroxyethylcarbamate

Chemical Property:

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Technology Process of tert-butyl 2-(3-chlorophenyl)-2-hydroxyethylcarbamate

There total 3 articles about tert-butyl 2-(3-chlorophenyl)-2-hydroxyethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 53360-89-7
2-amino-1-(3-chloro-phenyl)-ethanol

: 1187983-89-6
[2-(3-chloro-phenyl)-2-hydroxy-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: In tetrahydrofuran; for 1h;

Reference yield:

: 587-04-2
m-Chlorobenzaldehyde

: 1187983-89-6
[2-(3-chloro-phenyl)-2-hydroxy-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: potassium cyanide; acetic acid / methanol

2: lithium aluminium tetrahydride; sodium hydroxide / tetrahydrofuran

3: tetrahydrofuran

With potassium cyanide; sodium hydroxide; lithium aluminium tetrahydride; acetic acid; In tetrahydrofuran; methanol;

Reference yield:

: 97070-75-2,122047-10-3,137766-66-6,53313-92-1
2-(3-chlorophenyl)-2-hydroxyacetonitrile

: 1187983-89-6
[2-(3-chloro-phenyl)-2-hydroxy-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride; sodium hydroxide / tetrahydrofuran

2: tetrahydrofuran

With sodium hydroxide; lithium aluminium tetrahydride; In tetrahydrofuran;