3-Bromo-2-(bromomethyl)benzonitrile

Base Information

Chemical Name:3-Bromo-2-(bromomethyl)benzonitrile
CAS No.:1233479-42-9
Molecular Formula:C8H5Br2N
Molecular Weight:274.942
Hs Code.:2926909090
DSSTox Substance ID:DTXSID20596778
Wikidata:Q82492124
Mol file:1233479-42-9.mol

Synonyms:3-Bromo-2-(bromomethyl)benzonitrile;1233479-42-9;2-CYANO-6-BROMOBENZYLBROMIDE;MFCD18390220;Benzonitrile, 3-bromo-2-(bromomethyl)-;SCHEMBL2780319;DTXSID20596778;JGGHLJKQQVOMMG-UHFFFAOYSA-N;CL8699;AKOS016008235;AS-46079;SY244007;DB-339171;CS-0443179;EN300-186830;3-Bromo-2-(bromomethyl)benzonitrile, AldrichCPR;A890790

Suppliers and Price of 3-Bromo-2-(bromomethyl)benzonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Alichem
3-Bromo-2-(bromomethyl)benzonitrile
500mg
$ 847.60

Alichem
3-Bromo-2-(bromomethyl)benzonitrile
1g
$ 1534.70

Alichem
3-Bromo-2-(bromomethyl)benzonitrile
250mg
$ 480.00

American Custom Chemicals Corporation
3-BROMO-2-(BROMOMETHYL)BENZONITRILE 95.00%
5MG
$ 498.71

Chemcia Scientific
3-Bromo-2-bromomethyl-benzonitrile ＞97%
5 G
$ 525.00

Crysdot
3-Bromo-2-(bromomethyl)benzonitrile 95+%
5g
$ 632.00

TRC
3-Bromo-2-(bromomethyl)benzonitrile
500mg
$ 240.00

AK Scientific
3-Bromo-2-(bromomethyl)benzonitrile
5g
$ 751.00

Total 9 raw suppliers

Chemical Property of 3-Bromo-2-(bromomethyl)benzonitrile

Chemical Property:

PSA：23.79000
LogP:3.21568
Storage Temp.:2-8°C
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:274.87682
Heavy Atom Count:11
Complexity:172

Purity/Quality:

97% ^*data from raw suppliers

3-Bromo-2-(bromomethyl)benzonitrile ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C(=C1)Br)CBr)C#N

Technology Process of 3-Bromo-2-(bromomethyl)benzonitrile

There total 5 articles about 3-Bromo-2-(bromomethyl)benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.5%

: 52780-15-1
3'-bromo-2'-methylbenzonitrile

: 1233479-42-9
1-bromo-2-(bromomethyl)-3-cyanobenzene

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; at 80 ℃; for 16h;

Reference yield:

: 2-methyl-4-(1H-pyrazol-1-yl)benzonitrile

: 1233479-42-9
1-bromo-2-(bromomethyl)-3-cyanobenzene

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In acetonitrile; at 170 ℃; for 1h; Microwave irradiation;

Reference yield:

: C₁₂H₁₃BrO₄

: 1233479-42-9
1-bromo-2-(bromomethyl)-3-cyanobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium hydroxide / 0.03 h / 0 °C

2: 1,3,5-trichloro-2,4,6-triazine / 16 h / 20 °C

3: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 16 h / Reflux; Inert atmosphere

With ammonium hydroxide; N-Bromosuccinimide; 1,3,5-trichloro-2,4,6-triazine; dibenzoyl peroxide; In tetrachloromethane;
DOI:10.1016/j.bmcl.2010.12.034