(E)-2-Naphthalenecarbaldehyde O-acetyl oxime

Base Information

• Chemical Name: (E)-2-Naphthalenecarbaldehyde O-acetyl oxime
• CAS No.: 51874-01-2
• Molecular Formula: C₁₃H₁₁NO₂
• Molecular Weight: 213.236
• Mol file: 51874-01-2.mol

Synonyms:(E)-2-Naphthalenecarbaldehyde O-acetyl oxime;syn-2-Naphthaldoxime O-acetate

Chemical Property of (E)-2-Naphthalenecarbaldehyde O-acetyl oxime

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (E)-2-Naphthalenecarbaldehyde O-acetyl oxime

There total 1 articles about (E)-2-Naphthalenecarbaldehyde O-acetyl oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(E)-2-naphthaldehyde oxime (51873-98-4) + acetyl chloride (75-36-5) → (E)-2-naphthaldoxime O-acetate (51874-01-2)

Guidance literature:

(E)-2-naphthaldehyde oxime; acetyl chloride; With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 5h; Inert atmosphere;

acetyl chloride; With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

DOI:10.1002/asia.201600085

Reference yield: 87.0%

(E)-2-naphthaldoxime O-acetate (51874-01-2) → 2-naphthalenecarbonitrile (613-46-7)

Guidance literature:

With iron(III) trifluoromethanesulfonate; In toluene; at 120 ℃; for 0.5h; Reagent/catalyst; Inert atmosphere; Green chemistry;

DOI:10.1002/asia.201600085

upstream raw materials:

(E)-2-naphthaldehyde oxime

acetyl chloride

Downstream raw materials:

2-naphthalenecarbonitrile

Refernces