tert-butyl 3-((methoxycarbonyl)methyl)-4-oxopiperidine-1-carboxylate

Base Information

Chemical Name:tert-butyl 3-((methoxycarbonyl)methyl)-4-oxopiperidine-1-carboxylate
CAS No.:694450-89-0
Molecular Formula:
Molecular Weight:271.31
Hs Code.:
Mol file:694450-89-0.mol

Synonyms:tert-butyl 3-((methoxycarbonyl)methyl)-4-oxopiperidine-1-carboxylate;tert-butyl 3-(2-methoxy-2-oxoethyl)-4-oxopiperidine-1-carboxylate

Suppliers and Price of tert-butyl 3-((methoxycarbonyl)methyl)-4-oxopiperidine-1-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of tert-butyl 3-((methoxycarbonyl)methyl)-4-oxopiperidine-1-carboxylate

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl 3-((methoxycarbonyl)methyl)-4-oxopiperidine-1-carboxylate

There total 2 articles about tert-butyl 3-((methoxycarbonyl)methyl)-4-oxopiperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96-32-2
bromoacetic acid methyl ester

: 207691-65-4
N-tert-butoxycarbonyl-4-(tetrahydropyrrole-1-yl)-1,2,3,6-tetrahydropyridine

: 694450-89-0
C₁₃H₂₁NO₅

: 1323999-43-4
C₁₇H₃₀N₂O₄

Guidance literature:: N-tert-butoxycarbonyl-4-(tetrahydropyrrole-1-yl)-1,2,3,6-tetrahydropyridine; With acetic acid; In tetrahydrofuran;

bromoacetic acid methyl ester; With zinc; In tetrahydrofuran; at 5 ℃;
DOI:10.1021/op2001723

Reference yield:

: 79099-07-3
N-tert-butyloxycarbonylpiperidin-4-one

: 694450-89-0
C₁₃H₂₁NO₅

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 3 h / Reflux; azeotropic dehydration; Large scale reaction

2.1: acetic acid / tetrahydrofuran

2.2: 5 °C

With acetic acid; In tetrahydrofuran;
DOI:10.1021/op2001723