1H-1,2,3-TRIAZOLO[4,5-B]PYRIDINE, 6-CHLORO-

Base Information

• Chemical Name: 1H-1,2,3-TRIAZOLO[4,5-B]PYRIDINE, 6-CHLORO-
• CAS No.: 408314-14-7
• Molecular Formula: C₅H₃ClN₄
• Molecular Weight: 154.559
• Hs Code.: 2933990090
• Mol file: 408314-14-7.mol

Synonyms:1H-1,2,3-TRIAZOLO[4,5-B]PYRIDINE, 6-CHLORO-;6-Chloro-1H-[1,2,3]triazolo[4,5-b]pyridine;6-chloro-3H-[1,2,3]triazolo[4,5-b]pyridine

Chemical Property of 1H-1,2,3-TRIAZOLO[4,5-B]PYRIDINE, 6-CHLORO-

Chemical Property:

• PSA: 54.46000
• LogP: 1.00630
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

6-Chloro-1H-[1,2,3]triazolo[4,5-b]pyridine 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-1,2,3-TRIAZOLO[4,5-B]PYRIDINE, 6-CHLORO-

There total 2 articles about 1H-1,2,3-TRIAZOLO[4,5-B]PYRIDINE, 6-CHLORO- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-amino-5-chloro-3-nitropyridine (5409-39-2) → 6-chloro-1H-[1,2,3]triazolo[4,5-b]pyridine (408314-14-7)

Guidance literature:

Multi-step reaction with 2 steps

1: Na₂S₂O₄; H₂O

2: Diazotization

With sodium dithionite; water;

DOI:10.1021/ja01173a527

Reference yield:

5-chloro-2,3-diaminopyridine (25710-20-7) → 6-chloro-1H-[1,2,3]triazolo[4,5-b]pyridine (408314-14-7)

Guidance literature:

Diazotization;

DOI:10.1021/ja01173a527

Reference yield:

6-chloro-1H-[1,2,3]triazolo[4,5-b]pyridine (408314-14-7) → v-triazolo<4,5-b>pyridine (273-34-7)

Guidance literature:

With sodium hydroxide; palladium on activated charcoal; platinum on activated charcoal; Hydrogenation;

DOI:10.1021/ja01173a527

upstream raw materials:

5-chloro-2,3-diaminopyridine

2-amino-5-chloro-3-nitropyridine

Downstream raw materials:

v-triazolo<4,5-b>pyridine

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