3,4-Dihydro-6-methoxy-2-phenyl-1-[4-(phenylmethoxy)phenyl]naphthalene

Base Information

• Chemical Name: 3,4-Dihydro-6-methoxy-2-phenyl-1-[4-(phenylmethoxy)phenyl]naphthalene
• CAS No.: 308812-06-8
• Molecular Formula: C30H26O2
• Molecular Weight: 418.535
• Mol file: 308812-06-8.mol

Synonyms:3,4-Dihydro-6-methoxy-2-phenyl-1-[4-(phenylmethoxy)phenyl]naphthalene

Chemical Property of 3,4-Dihydro-6-methoxy-2-phenyl-1-[4-(phenylmethoxy)phenyl]naphthalene

Chemical Property:

• Boiling Point: 570.3±50.0 °C(Predicted)
• PSA: 18.46000
• Density: 1.154±0.06 g/cm3(Predicted)
• LogP: 7.17950
• Storage Temp.: Refrigerator
• Solubility.: DMSO (Slightly, Heated), Ethyl Acetate (Slightly)

Purity/Quality:

97% ^*data from raw suppliers

3,4-Dihydro-6-methoxy-2-phenyl-1-[4-(phenylmethoxy)phenyl]naphthalene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,4-Dihydro-6-methoxy-2-phenyl-1-[4-(phenylmethoxy)phenyl]naphthalene

There total 3 articles about 3,4-Dihydro-6-methoxy-2-phenyl-1-[4-(phenylmethoxy)phenyl]naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-methoxy-3,4-dihydro-1(2H)-naphthalenone (1078-19-9) → 4-(4-(benzyloxy)phenyl)-7-methoxy-3-phenyl-1,2-dihydronaphthalene (308812-06-8)

Guidance literature:

Multi-step reaction with 2 steps

1.2: pyridinium tribromide

2.1: 71 percent / Pd(PPh₃)4 / tetrahydrofuran

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran;

DOI:10.1016/j.bmcl.2005.08.084

Reference yield:

(4-(benzyloxy)phenyl)magnesium bromide (120186-59-6) → 4-(4-(benzyloxy)phenyl)-7-methoxy-3-phenyl-1,2-dihydronaphthalene (308812-06-8)

Guidance literature:

Multi-step reaction with 2 steps

1.2: pyridinium tribromide

2.1: 71 percent / Pd(PPh₃)4 / tetrahydrofuran

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran;

DOI:10.1016/j.bmcl.2005.08.084

Reference yield:

p-benzyloxyphenylbromide (6793-92-6) → 4-(4-(benzyloxy)phenyl)-7-methoxy-3-phenyl-1,2-dihydronaphthalene (308812-06-8)

Guidance literature:

Multi-step reaction with 3 steps

1.1: iodine; magnesium / tetrahydrofuran / 0.75 h / 60 °C

1.2: 3 h / 40 - 65 °C

2.1: pyridinium hydrobromide perbromide / tetrahydrofuran / 3 h / 20 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / N,N-dimethyl-formamide / 3.5 h / 100 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; iodine; sodium carbonate; magnesium; pyridinium hydrobromide perbromide; In tetrahydrofuran; N,N-dimethyl-formamide;

upstream raw materials:

(4-(benzyloxy)phenyl)magnesium bromide

6-methoxy-3,4-dihydro-1(2H)-naphthalenone

p-benzyloxyphenylbromide

Downstream raw materials:

4-(6-methoxy-2-phenyl-1,2,3,4-tetrahydronaphthalen-1-yl)phenol

cis-4-(1,2,3,4-tetrahydro-6-methoxy-2-phenyl-1-naphthalenyl)phenol

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