1-Acetyl-6-chloro-1H-indole

Base Information

• Chemical Name: 1-Acetyl-6-chloro-1H-indole
• CAS No.: 126759-61-3
• Molecular Formula: C10H8ClNO
• Molecular Weight: 193.62962
• Mol file: 126759-61-3.mol

Synonyms:1-Acetyl-6-chloro-1H-indole

Chemical Property of 1-Acetyl-6-chloro-1H-indole

Chemical Property:

• PSA: 22.00000
• LogP: 2.95480

Purity/Quality:

98% ^*data from raw suppliers

1-(6-Chloro-1H-indol-1-yl)ethanone 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-Acetyl-6-chloro-1H-indole

There total 4 articles about 1-Acetyl-6-chloro-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

6-chloroindole (17422-33-2) + acetic anhydride (108-24-7) → 1-(6-chloroindol-1-yl)ethanone (126759-61-3)

Guidance literature:

With dmap; triethylamine; In DCE; at 60 ℃; for 24h;

DOI:10.1002/anie.200901072

Reference yield: 90.0%

6-chloroindole (17422-33-2) + acetyl chloride (75-36-5) → 1-(6-chloroindol-1-yl)ethanone (126759-61-3)

Guidance literature:

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate;

DOI:10.1080/00397919908085950

Reference yield: 64.0%

2-ethenyl-5-chloroacetanilide (126759-55-5) → 1-(6-chloroindol-1-yl)ethanone (126759-61-3)

Guidance literature:

With oxygen; copper(l) chloride; palladium dichloride; In 1,2-dimethoxyethane; under 760 Torr;

upstream raw materials:

2-ethenyl-5-chloroacetanilide

6-chloroindole

acetyl chloride

N-(2-bromo-5-chlorophenyl)acetamide

Downstream raw materials:

6-chloro-2-(2',4'-dimethoxyphenyl)-N-acetylindole

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