1-BOC-4-(3-CHLOROPHENYL)-4-PIPERIDINEDICARBOXYLIC ACID

Base Information

Chemical Name:1-BOC-4-(3-CHLOROPHENYL)-4-PIPERIDINEDICARBOXYLIC ACID
CAS No.:100112-49-0
Molecular Formula:C₂₇H₃₀ClNO₄
Molecular Weight:0
Hs Code.:

Synonyms:1-(TERT-BUTOXYCARBONYL)-4-(3-CHLOROPHENYL)PIPERIDINE-4-CARBOXYLIC ACID;1-BOC-4-(3-CHLOROPHENYL)-4-PIPERIDINEDICARBOXYLIC ACID;N-BOC-4-(M-CHLOROPHENYL)-4-PIPERIDINECARBOXYLIC ACID;1-Boc-4-(3-chlorophenyl)-4-carboxypiperidine

Suppliers and Price of 1-BOC-4-(3-CHLOROPHENYL)-4-PIPERIDINEDICARBOXYLIC ACID

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-BOC-4-(3-CHLOROPHENYL)-4-PIPERIDINEDICARBOXYLIC ACID

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-BOC-4-(3-CHLOROPHENYL)-4-PIPERIDINEDICARBOXYLIC ACID

There total 2 articles about 1-BOC-4-(3-CHLOROPHENYL)-4-PIPERIDINEDICARBOXYLIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100112-46-7
3,4-bis-(benzyloxy)-ω-(isopropulamino)acetophenone hydrobromide

: 100112-49-0
N-[2-(3,4-Bis-benzyloxy-phenyl)-2-hydroxy-ethyl]-2-chloro-N-isopropyl-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / LiAlH₄ / diethyl ether / 4 h / Heating

2: Et₃N / CHCl₃ / 4 h / Ambient temperature

With lithium aluminium tetrahydride; triethylamine; In diethyl ether; chloroform;
DOI:10.1021/jm00155a025

Reference yield:

: 100112-47-8
1-<3,4-bis-(benzyloxy)phenyl>-2-(isopropulamino)ethanol

: 79-04-9
chloroacetyl chloride

: 100112-49-0
N-[2-(3,4-Bis-benzyloxy-phenyl)-2-hydroxy-ethyl]-2-chloro-N-isopropyl-acetamide

Guidance literature:: With triethylamine; In chloroform; for 4h; Ambient temperature;
DOI:10.1021/jm00155a025

Reference yield:

: 100112-49-0
N-[2-(3,4-Bis-benzyloxy-phenyl)-2-hydroxy-ethyl]-2-chloro-N-isopropyl-acetamide

: 100112-62-7
2-(3,4-dihydroxyphenyl)-4-isopropylmorpholine

Guidance literature:: Multi-step reaction with 3 steps

1: KOH / ethanol / 30 h / Ambient temperature

2: 34 percent / NaBH₄, BF₃*Et₂O / tetrahydrofuran / 1.5 h / Heating

3: H₂ / 10percent Pd/C / CHCl₃; ethanol

With potassium hydroxide; sodium tetrahydroborate; boron trifluoride diethyl etherate; hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1021/jm00155a025