4-broMo-2-cyanobenzene-1-sulfonyl chloride

Base Information

Chemical Name:4-broMo-2-cyanobenzene-1-sulfonyl chloride
CAS No.:1261583-46-3
Molecular Formula:C7H3BrClNO2S
Molecular Weight:280.529
Hs Code.:
Mol file:1261583-46-3.mol

Synonyms:4-broMo-2-cyanobenzene-1-sulfonyl chloride;4-Bromo-3-cyanobenzene-1-sulfonyl chloride

Suppliers and Price of 4-broMo-2-cyanobenzene-1-sulfonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-Bromo-3-cyanobenzene-1-sulfonylChloride
100mg
$ 155.00

Crysdot
4-Bromo-3-cyanobenzene-1-sulfonylchloride 95+%
1g
$ 430.00

Crysdot
4-Bromo-3-cyanobenzene-1-sulfonylchloride 95+%
250mg
$ 200.00

Alichem
4-Bromo-3-cyanobenzene-1-sulfonylchloride
5g
$ 959.50

Abosyn
4-bromo-3-cyanobenzene-1-sulfonylchloride 95%-98%
1g
$ 807.00

Total 6 raw suppliers

Chemical Property of 4-broMo-2-cyanobenzene-1-sulfonyl chloride

Chemical Property:

Boiling Point:366.2±32.0 °C(Predicted)
PSA：66.31000
Density:1.94±0.1 g/cm3(Predicted)
LogP:3.32908

Purity/Quality:

97% ^*data from raw suppliers

4-Bromo-3-cyanobenzene-1-sulfonylChloride ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-broMo-2-cyanobenzene-1-sulfonyl chloride

There total 1 articles about 4-broMo-2-cyanobenzene-1-sulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 72115-09-4
5-amino-2-bromo-benzonitrile

: 1261583-46-3
4-bromo-3-cyanobenzene-1-sulfonyl chloride

Guidance literature:: 5-amino-2-bromo-benzonitrile; With hydrogenchloride; acetic acid; at 0 ℃; for 0.166667h;

With sodium nitrite; In water; at 0 ℃; for 0.333333h; Further stages;

Reference yield: 73.0%

: 1063733-41-4
N-[(2,4-dimethoxyphenyl)methyl]-1,2,4-thiadiazol-5-amine

: 1261583-46-3
4-bromo-3-cyanobenzene-1-sulfonyl chloride

: 1354917-87-5
4-bromo-3-cyano-N-(2,4-dimethoxybenzyl)-N-1,2,4-thiadiazol-5-ylbenzenesulfonamide

Guidance literature:: N-[(2,4-dimethoxyphenyl)methyl]-1,2,4-thiadiazol-5-amine; With lithium bis(trimethylsilyl)azanide; In tetrahydrofuran; at -78 ℃; for 0.25h; Inert atmosphere;

4-bromo-3-cyanobenzene-1-sulfonyl chloride; In tetrahydrofuran; at 20 ℃; for 3h;

Reference yield: 73.0%

: 1261583-46-3
4-bromo-3-cyanobenzene-1-sulfonyl chloride

: tert-butyl 5-[(4-methoxyphenyl)methylamino]thiazole-4-carboxylate

: tert-butyl 5-{N-[(4-methoxyphenyl)methyl]4-bromo-3-cyanobenzenesulfonamido}-1,3-thiazole-4-carboxylate

Guidance literature:: tert-butyl 5-[(4-methoxyphenyl)methylamino]thiazole-4-carboxylate; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 0.5h; Inert atmosphere;

4-bromo-3-cyanobenzene-1-sulfonyl chloride; In tetrahydrofuran; at 0 - 20 ℃; for 0.5h; Inert atmosphere;