(7-Methoxy-1,2,3,4-tetrahydronaphthalen-2-yl)-propylazanium;chloride

Base Information

• Chemical Name: (7-Methoxy-1,2,3,4-tetrahydronaphthalen-2-yl)-propylazanium;chloride
• CAS No.: 93601-93-5
• Molecular Formula: C₁₄H₂₁NO*ClH
• Molecular Weight: 255.788
• Mol file: 93601-93-5.mol

Synonyms:(7-methoxy-1,2,3,4-tetrahydronaphthalen-2-yl)-propylazanium;chloride

Chemical Property of (7-Methoxy-1,2,3,4-tetrahydronaphthalen-2-yl)-propylazanium;chloride

Chemical Property:

• PSA: 21.26000
• LogP: 3.74500
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 255.1389920
• Heavy Atom Count: 17
• Complexity: 207

Purity/Quality:

(7-METHOXY-1,2,3,4-TETRAHYDRONAPHTHALEN-2-YL)(PROPYL)AMINE HYDROCHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCC[NH2+]C1CCC2=C(C1)C=C(C=C2)OC.[Cl-]

Technology Process of (7-Methoxy-1,2,3,4-tetrahydronaphthalen-2-yl)-propylazanium;chloride

There total 2 articles about (7-Methoxy-1,2,3,4-tetrahydronaphthalen-2-yl)-propylazanium;chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

propylamine (107-10-8,42939-71-9) + 7-methoxyl-2-tetralone (4133-34-0) → (7-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-propylamine hydrochloride (93601-93-5)

Guidance literature:

With hydrogenchloride; sodium tris(acetoxy)borohydride; In 1,1-dichloroethane;

Reference yield:

(7-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-propyl-amine (148258-42-8) → (7-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-propylamine hydrochloride (93601-93-5)

Guidance literature:

With hydrogenchloride; In diethyl ether; ethyl acetate;

DOI:10.1021/jm901618d

Reference yield: 53.5%

2-chloro-1-(4-(4-(pyridin-3-yl)phenyl)piperazin-1-yl)ethanone (1245728-34-0) + (7-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-propylamine hydrochloride (93601-93-5) → 2-((7-methoxy-1,2,3,4-tetrahydronaphthalen-2-yl)(propyl)amino)-1-(4-(4-(pyridin-3-yl)phenyl)piperazin-1-yl)ethanone (1245728-36-2)

Guidance literature:

With potassium carbonate; In acetonitrile; for 1h; Reflux;

DOI:10.1016/j.bmc.2010.06.025

upstream raw materials:

propylamine

7-methoxyl-2-tetralone

(7-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-propyl-amine

Downstream raw materials:

(R)-7-methoxy-2-(n-propylamino)tetralin

(S)-7-methoxy-N-propyl-1,2,3,4-tetrahydronaphthalen-2-amine

N-{2-[(7-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-propyl-amino]-ethyl}-benzamide

(7-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-propyl-amine

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