4-BroMo-2-isopropoxybenzaldehyde

Base Information

• Chemical Name: 4-BroMo-2-isopropoxybenzaldehyde
• CAS No.: 1099672-01-1
• Molecular Formula: C10H11BrO2
• Molecular Weight: 243.09714
• Hs Code.: 2913000090
• Mol file: 1099672-01-1.mol

Synonyms:4-BroMo-2-isopropoxybenzaldehyde

Chemical Property of 4-BroMo-2-isopropoxybenzaldehyde

Chemical Property:

• PSA: 26.30000
• LogP: 3.04880
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

4-Bromo-2-isopropoxybenzaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 4-Bromo-2-isopropoxybenzaldehyde is used as a reactant in the preparation of dihydrobenzopyrans by hydride transfer initiated cyclization of ortho-vinylaryl alkyl ethers.

Technology Process of 4-BroMo-2-isopropoxybenzaldehyde

There total 3 articles about 4-BroMo-2-isopropoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

→ 4-bromo-2-isopropoxybenzaldehyde (1099672-01-1)

Guidance literature:

With potassium carbonate; In acetonitrile; at 70 ℃;

Reference yield: 34.0%

C10H13BrO2 (1099693-56-7) → 4-bromo-2-isopropoxybenzaldehyde (1099672-01-1)

Guidance literature:

With manganese(IV) oxide; In diethyl ether; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1021/ol900915p

Reference yield:

2-iodo-propane (75-30-9) + 4-bromosalicylaldehyde (22532-62-3) → 4-bromo-2-isopropoxybenzaldehyde (1099672-01-1)

Guidance literature:

With potassium carbonate; caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 8h; Inert atmosphere;

DOI:10.1021/jacs.8b05191

upstream raw materials:

C₁₀H₁₃BrO₂

2-iodo-propane

4-bromosalicylaldehyde

Downstream raw materials:

C₁₅H₁₇BrO₅