2-[3-(2-nitrophenoxy)-2-oxopropyl]-1H-isoindole-1,3(2H)-dione

Base Information

Chemical Name:2-[3-(2-nitrophenoxy)-2-oxopropyl]-1H-isoindole-1,3(2H)-dione
CAS No.:54252-53-8
Molecular Formula:C17H12N2O6
Molecular Weight:340.292
Hs Code.:
NSC Number:173315
DSSTox Substance ID:DTXSID40306018
Wikidata:Q82052886

Synonyms:54252-53-8;NSC173315;DTXSID40306018;NSC-173315;2-[3-(2-nitrophenoxy)-2-oxopropyl]-1H-isoindole-1,3(2H)-dione

Suppliers and Price of 2-[3-(2-nitrophenoxy)-2-oxopropyl]-1H-isoindole-1,3(2H)-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 2-[3-(2-nitrophenoxy)-2-oxopropyl]-1H-isoindole-1,3(2H)-dione

Chemical Property:

Vapor Pressure:7.81E-12mmHg at 25°C
Boiling Point:542.6°Cat760mmHg
Flash Point:281.9°C
Density:1.454g/cm³
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:5
Exact Mass:340.06953611
Heavy Atom Count:25
Complexity:548

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C(=O)N(C2=O)CC(=O)COC3=CC=CC=C3[N+](=O)[O-]

Technology Process of 2-[3-(2-nitrophenoxy)-2-oxopropyl]-1H-isoindole-1,3(2H)-dione

There total 5 articles about 2-[3-(2-nitrophenoxy)-2-oxopropyl]-1H-isoindole-1,3(2H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 54252-49-2
2-[2-hydroxy-3-(2-nitrophenoxy)propyl]isoindole-1,3-dione

: 54252-53-8
2-[3-(2-nitrophenoxy)-2-oxypropyl]isoindole-1,3-dione

Guidance literature:: With Dess-Martin periodane; In dichloromethane; dimethyl sulfoxide; at 60 ℃; for 3h;
DOI:10.1021/jm0307741

Reference yield:

: 21407-49-8
2-nitrophenyl glycidyl ether

: 54252-53-8
2-[3-(2-nitrophenoxy)-2-oxypropyl]isoindole-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / pyridine / butan-1-ol / 16 h / Heating

2: 87 percent / Dess-Martin periodinane / CH₂Cl₂; dimethylsulfoxide / 3 h / 60 °C

With pyridine; Dess-Martin periodane; In dichloromethane; dimethyl sulfoxide; butan-1-ol;
DOI:10.1021/jm0307741

Reference yield:

: 136918-14-4,85-41-6
phthalimide

: 54252-53-8
2-[3-(2-nitrophenoxy)-2-oxypropyl]isoindole-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / pyridine / butan-1-ol / 16 h / Heating

2: 87 percent / Dess-Martin periodinane / CH₂Cl₂; dimethylsulfoxide / 3 h / 60 °C

With pyridine; Dess-Martin periodane; In dichloromethane; dimethyl sulfoxide; butan-1-ol;
DOI:10.1021/jm0307741