3-Iodo-1-nitronaphthalene

Base Information

• Chemical Name: 3-Iodo-1-nitronaphthalene
• CAS No.: 690226-82-5
• Molecular Formula: C10H6INO2
• Molecular Weight: 299.06461
• DSSTox Substance ID: DTXSID70704785
• Wikidata: Q82637334
• Mol file: 690226-82-5.mol

Synonyms:3-Iodo-1-nitronaphthalene;690226-82-5;DTXSID70704785;FT-0759723;F77265

Chemical Property of 3-Iodo-1-nitronaphthalene

Chemical Property:

• PSA: 45.82000
• LogP: 3.87580
• XLogP3: 3.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 298.94433
• Heavy Atom Count: 14
• Complexity: 229

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C=C(C=C2[N+](=O)[O-])I

Technology Process of 3-Iodo-1-nitronaphthalene

There total 4 articles about 3-Iodo-1-nitronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 3-iodo-1-nitro-naphthalene (690226-82-5)

Guidance literature:

With bromine; at 130 - 160 ℃;

DOI:10.1039/jr9310003176

Reference yield:

2-iodo-4-nitronaphthalen-1-ylamine (53870-84-1) → 3-iodo-1-nitro-naphthalene (690226-82-5)

Guidance literature:

With sulfuric acid; acetic acid; sodium nitrite; Behandlung der Diazoniumsalz-Loesung mit Aethanol unter Erwaermen;

DOI:10.1039/jr9340001705

Reference yield:

1-amino-4-nitronaphthalene (776-34-1) → 3-iodo-1-nitro-naphthalene (690226-82-5)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid; iodine monochloride

2: ethanolic H₂SO₄ / anschliessendes Kochen

With sulfuric acid; Iodine monochloride; acetic acid;

DOI:10.1039/jr9310003176

upstream raw materials:

2-iodo-4-nitronaphthalen-1-ylamine

isopentyl nitrite

1-amino-4-nitronaphthalene

Downstream raw materials:

3-iodo-1-naphthol

3-iodo-[1]naphthylamine