N-ISOPROPYL-4-FLUORO-2-NITROANILINE

Base Information

• Chemical Name: N-ISOPROPYL-4-FLUORO-2-NITROANILINE
• CAS No.: 146366-00-9
• Molecular Formula: C9H11FN2O2
• Molecular Weight: 198.197
• Hs Code.: 2921420090
• Mol file: 146366-00-9.mol

Synonyms:BUTTPARK 45\09-83;N-ISOPROPYL-4-FLUORO-2-NITROANILINE;N-(4-Fluoro-2-nitrophenyl)-N-isopropylamine

Chemical Property of N-ISOPROPYL-4-FLUORO-2-NITROANILINE

Chemical Property:

• PSA: 57.85000
• LogP: 3.15040

Purity/Quality:

99% ^*data from raw suppliers

4-Fluoro-2-nitro-N-(propan-2-yl)aniline ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

Useful:

Technology Process of N-ISOPROPYL-4-FLUORO-2-NITROANILINE

There total 2 articles about N-ISOPROPYL-4-FLUORO-2-NITROANILINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,4-difluoro-2-nitrobenzene (364-74-9) + isopropylamine (75-31-0) → 4-Fluoro-N-(1-methylethyl)-2-nitrobenzenamine (146366-00-9)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; for 18h; Inert atmosphere;

DOI:10.1021/jm900888c

Reference yield:

2-nitro-4-fluoroaniline (364-78-3) + 2,2-dimethoxy-propane (77-76-9) → 4-Fluoro-N-(1-methylethyl)-2-nitrobenzenamine (146366-00-9)

Guidance literature:

With borane pyridine; trifluoroacetic acid; Multistep reaction; 1.) toluene, 2.) toluene;

DOI:10.1021/jm981098j

Reference yield:

4-Fluoro-N-(1-methylethyl)-2-nitrobenzenamine (146366-00-9) → 4-fluoro-N1-isopropyl-benzene-1,2-diamine (153877-87-3)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; at 20 ℃; under 2280 Torr;

DOI:10.1021/jm981098j

upstream raw materials:

2-nitro-4-fluoroaniline

2,2-dimethoxy-propane

1,4-difluoro-2-nitrobenzene

isopropylamine

Downstream raw materials:

4-fluoro-N¹-isopropyl-benzene-1,2-diamine

5-fluoro-1-isopropyl-1,3-dihydro-2H-benzimidazol-2-one

1,3-dihydro-5-fluoro-1-(1-methylethyl)-6-nitro-2H-benzimidazol-2-one

6-fluoro-3-isopropyl-5-nitro-2-oxo-2,3-dihydro-benzoimidazole-1-carboxylic acid (2-chloro-ethyl)-amide

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