5‐bromo‐2‐(methylsulfanyl)pyrrolo[2,1‐ f][1,2,4]triazine

Base Information

Chemical Name:5‐bromo‐2‐(methylsulfanyl)pyrrolo[2,1‐ f][1,2,4]triazine
CAS No.:1233181-67-3
Molecular Formula:
Molecular Weight:0
Hs Code.:
Mol file:1233181-67-3.mol

Synonyms:5‐bromo‐2‐(methylsulfanyl)pyrrolo[2,1‐ f][1,2,4]triazine;5-Bromo-2-(methylthio)pyrrolo[2,1-f][1,2,4]triazine

Suppliers and Price of 5‐bromo‐2‐(methylsulfanyl)pyrrolo[2,1‐ f][1,2,4]triazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 6 raw suppliers

Chemical Property of 5‐bromo‐2‐(methylsulfanyl)pyrrolo[2,1‐ f][1,2,4]triazine

Chemical Property:

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5‐bromo‐2‐(methylsulfanyl)pyrrolo[2,1‐ f][1,2,4]triazine

There total 4 articles about 5‐bromo‐2‐(methylsulfanyl)pyrrolo[2,1‐ f][1,2,4]triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1120214-78-9
4-chloro-2-methylsulfanyl-pyrrolo[2,1-f][1,2,4]triazine

: 1233094-95-5
7-bromo-2-methylsulfanyl-pyrrolo[2,1-f][1,2,4]triazine

: 1233181-67-3
5-bromo-2-methylsulfanyl-pyrrolo[2,1-f][1,2,4]triazine

: 1232815-52-9
5,7-dibromo-2-methylsulfanyl-pyrrolo[2,1-f][1,2,4]triazine

Guidance literature:: 4-chloro-2-methylsulfanyl-pyrrolo[2,1-f][1,2,4]triazine; With N-Bromosuccinimide; In tetrahydrofuran; methanol; at 0 - 24 ℃; for 2h;

With sodium tetrahydroborate; In isopropyl alcohol; at 60 ℃; for 3h;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; for 0.75h;
DOI:10.1021/ol2015237

Reference yield:

: 1232815-48-3
1-(3-benzoyl-thioureido)-1H-pyrrole-2-carboxylic acid methyl ester

: 1233094-95-5
7-bromo-2-methylsulfanyl-pyrrolo[2,1-f][1,2,4]triazine

: 1233181-67-3
5-bromo-2-methylsulfanyl-pyrrolo[2,1-f][1,2,4]triazine

: 1232815-52-9
5,7-dibromo-2-methylsulfanyl-pyrrolo[2,1-f][1,2,4]triazine

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide / water / 1.25 h / 85 °C

2.1: tetrahydrofuran / 1 h / 45 °C

3.1: trichlorophosphate / 4 h / 100 °C

4.1: N-Bromosuccinimide / tetrahydrofuran; methanol / 2 h / 0 - 24 °C

4.2: 3 h / 60 °C

4.3: 0.75 h

With N-Bromosuccinimide; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; methanol; water;
DOI:10.1021/ol2015237

Reference yield:

: 1232815-49-4
2-thioxo-2,3-dihydro-1H-pyrrolo[2,1-f][1,2,4]triazin-4-one

: 1233094-95-5
7-bromo-2-methylsulfanyl-pyrrolo[2,1-f][1,2,4]triazine

: 1233181-67-3
5-bromo-2-methylsulfanyl-pyrrolo[2,1-f][1,2,4]triazine

: 1232815-52-9
5,7-dibromo-2-methylsulfanyl-pyrrolo[2,1-f][1,2,4]triazine

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 1 h / 45 °C

2.1: trichlorophosphate / 4 h / 100 °C

3.1: N-Bromosuccinimide / tetrahydrofuran; methanol / 2 h / 0 - 24 °C

3.2: 3 h / 60 °C

3.3: 0.75 h

With N-Bromosuccinimide; trichlorophosphate; In tetrahydrofuran; methanol;
DOI:10.1021/ol2015237