1-Naphthylhydroxylamine

Base Information

• Chemical Name: 1-Naphthylhydroxylamine
• CAS No.: 607-30-7
• Molecular Formula: C10H9 N O
• Molecular Weight: 159.188
• Hs Code.: 2928000090
• UNII: 5O045G232P
• DSSTox Substance ID: DTXSID40209510
• Nikkaji Number: J2.985H
• Wikidata: Q26840867
• Metabolomics Workbench ID: 55041
• ChEMBL ID: CHEMBL261899
• Mol file: 607-30-7.mol

Synonyms:1-naphthylhydroxylamine;N-hydroxy-1-naphthylamine

Chemical Property of 1-Naphthylhydroxylamine

Chemical Property:

• Vapor Pressure: 3.47E-05mmHg at 25°C
• Melting Point: 79°C
• Refractive Index: 1.5460 (estimate)
• Boiling Point: 339.8°C at 760 mmHg
• PKA: 9.00±0.30(Predicted)
• Flash Point: 174.9°C
• PSA: 32.26000
• Density: 1.283g/cm³
• LogP: 2.71390
• XLogP3: 2.4
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 159.068413911
• Heavy Atom Count: 12
• Complexity: 149

Purity/Quality:

98%min ^*data from raw suppliers

N-HYDROXY-1-NAPHTHYLAMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Chemical Classes: Nitrogen Compounds -> Naphthylamines
• Canonical SMILES: C1=CC=C2C(=C1)C=CC=C2NO

Technology Process of 1-Naphthylhydroxylamine

There total 2 articles about 1-Naphthylhydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1-Nitronaphthalene (86-57-7) → hydroxynaphthylamine (607-30-7,77635-08-6)

Guidance literature:

With sodium tetrahydroborate; palladium diacetate; In ethanol; dichloromethane; water; at 20 ℃; for 0.0666667h;

DOI:10.1039/c9gc03957k

Reference yield:

→ hydroxynaphthylamine (607-30-7,77635-08-6)

Guidance literature:

DOI:10.1039/c19660000464 DOI:10.1021/jo00925a037

Reference yield: 37.0%

hydroxynaphthylamine (607-30-7,77635-08-6) + phenylacetylene (536-74-3) → 3-phenyl-1H-benzo[g]indole (569344-73-6)

Guidance literature:

With iron(II) phthalocyanine; In toluene; regioselective reaction; Reflux; Inert atmosphere;

DOI:10.1016/j.tet.2009.03.004

upstream raw materials:

1-Nitronaphthalene

Downstream raw materials:

1,4-Dihydroxynaphthalene

4-amino-1-naphthol

4-amino-1-naphthalenesufonic acid

1-naphthylsulfamic acid