6-Bromo-1-methyl-2-oxo-1,2,3,4-tetrahydroquinoline

Base Information

Chemical Name:6-Bromo-1-methyl-2-oxo-1,2,3,4-tetrahydroquinoline
CAS No.:1092523-03-9
Molecular Formula:C10H10BrNO
Molecular Weight:240.099
Hs Code.:2933790090
Mol file:1092523-03-9.mol

Synonyms:6-Bromo-1-methyl-2-oxo-1,2,3,4-tetrahydroquinoline;6-Bromo-3,4-dihydro-1-methylquinolin-2(1H)-one;6-bromo-3,4-dihydro-1-methyl-2(1H)-Quinolinone

Suppliers and Price of 6-Bromo-1-methyl-2-oxo-1,2,3,4-tetrahydroquinoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
6-Bromo-1-methyl-1,2,3,4-tetrahydroquinolin-2-one
500mg
$ 265.00

SynQuest Laboratories
6-Bromo-3,4-dihydro-1-methylquinolin-2(1H)-one
5 g
$ 992.00

SynQuest Laboratories
6-Bromo-3,4-dihydro-1-methylquinolin-2(1H)-one
1 g
$ 240.00

Matrix Scientific
6-Bromo-1-methyl-1,2,3,4-tetrahydroquinolin-2-one >97%
1g
$ 279.00

Matrix Scientific
6-Bromo-1-methyl-1,2,3,4-tetrahydroquinolin-2-one >97%
500mg
$ 177.00

Crysdot
6-Bromo-1-methyl-3,4-dihydroquinolin-2(1H)-one 95+%
5g
$ 795.00

Chemenu
6-Bromo-1-methyl-3,4-dihydroquinolin-2(1H)-one 95%
5g
$ 743.00

Apolloscientific
6-Bromo-3,4-dihydro-1-methylquinolin-2(1H)-one
5g
$ 837.00

Alichem
6-Bromo-1-methyl-1,2,3,4-tetrahydroquinolin-2-one
5g
$ 826.80

AK Scientific
6-Bromo-1-methyl-1,2,3,4-tetrahydroquinolin-2-one
500mg
$ 235.00

Total 12 raw suppliers

Chemical Property of 6-Bromo-1-methyl-2-oxo-1,2,3,4-tetrahydroquinoline

Chemical Property:

Boiling Point:429.2±45.0 °C(Predicted)
PKA:0.33±0.20(Predicted)
PSA：20.31000
Density:1.500±0.06 g/cm3(Predicted)
LogP:2.42310
Storage Temp.:Sealed in dry,Room Temperature

Purity/Quality:

99%, ^*data from raw suppliers

6-Bromo-1-methyl-1,2,3,4-tetrahydroquinolin-2-one ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-Bromo-1-methyl-2-oxo-1,2,3,4-tetrahydroquinoline

There total 3 articles about 6-Bromo-1-methyl-2-oxo-1,2,3,4-tetrahydroquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 3279-90-1
6-bromo-3,4-dihydro-1H-quinolin-2-one

: 74-88-4
methyl iodide

: 1092523-03-9
6-bromo-1-methyl-3,4-dihydroquinolin-2(1H)-one

Guidance literature:: 6-bromo-3,4-dihydro-1H-quinolin-2-one; With potassium tert-butylate; In N,N-dimethyl-formamide; at 0 ℃; for 0.25h;

methyl iodide; In N,N-dimethyl-formamide; at 0 - 20 ℃;

Reference yield:

: 3279-90-1
6-bromo-3,4-dihydro-1H-quinolin-2-one

: 77-78-1
dimethyl sulfate

: 1092523-03-9
6-bromo-1-methyl-3,4-dihydroquinolin-2(1H)-one

Guidance literature:: 6-bromo-3,4-dihydro-1H-quinolin-2-one; With sodium hydride; In toluene; mineral oil; at 0 - 20 ℃; for 0.5h;

dimethyl sulfate; In toluene; mineral oil; at 60 ℃; for 1h;

Reference yield:

: 553-03-7
3,4-dihydro-2(1H)-quinolone

: 1092523-03-9
6-bromo-1-methyl-3,4-dihydroquinolin-2(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / N,N-dimethyl-formamide / 2 h / 0 °C

2: potassium tert-butylate / N,N-dimethyl-formamide / 0.5 h / 20 °C

With N-Bromosuccinimide; potassium tert-butylate; In N,N-dimethyl-formamide;