2-Methylbenzo[d]thiazol-6-ylboronic acid pinacol ester

Base Information

Chemical Name:2-Methylbenzo[d]thiazol-6-ylboronic acid pinacol ester
CAS No.:837392-69-5
Molecular Formula:C14H20BNO3S
Molecular Weight:275.179
Hs Code.:
Mol file:837392-69-5.mol

Synonyms:2-Methylbenzo[d]thiazol-6-ylboronic acid pinacol ester;2-methyl-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzo[d]thiazole

Suppliers and Price of 2-Methylbenzo[d]thiazol-6-ylboronic acid pinacol ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-Methylbenzo[d]thiazol-6-ylboronic acid pinacol ester

Chemical Property:

PSA：59.59000
LogP:2.90390

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Methylbenzo[d]thiazol-6-ylboronic acid pinacol ester

There total 3 articles about 2-Methylbenzo[d]thiazol-6-ylboronic acid pinacol ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 5304-21-2
6-bromo-2-methylbenzothiazole

: 73183-34-3
bis(pinacol)diborane

: 837392-69-5
2-methyl-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzo[d]thiazole

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; C₄₀H₂₉P; potassium acetate; In 2-methyltetrahydrofuran; at 90 ℃; for 24h; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.9b02414

Reference yield: 90.0%

: 837392-69-5
2-methyl-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzo[d]thiazole

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In N,N-dimethyl-formamide; at 80 ℃; for 24h; Inert atmosphere;

Reference yield: 24.0%

: 120-75-2
2-Methylbenzothiazole

: 73183-34-3
bis(pinacol)diborane

: 1573171-26-2
2-methylbenzothiazole-7-boronic acid pinacol ester

: 837392-69-5
2-methyl-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzo[d]thiazole

Guidance literature:: With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 3,4,7,8-Tetramethyl-o-phenanthrolin; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere; Glovebox;
DOI:10.1021/ja412563e