2-Methyl-3,4-dichloropyridine N-oxide

Base Information

Chemical Name:2-Methyl-3,4-dichloropyridine N-oxide
CAS No.:108004-98-4
Molecular Formula:C₆H₅Cl₂NO
Molecular Weight:178.018
Hs Code.:
DSSTox Substance ID:DTXSID00546635
Wikidata:Q82424525
Mol file:108004-98-4.mol

Synonyms:2-METHYL-3,4-DICHLOROPYRIDINE N-OXIDE;108004-98-4;3,4-dichloro-2-methyl-1-oxidopyridin-1-ium;3,4-Dichloro-2-methylpyridine 1-oxide;starbld0002039;SCHEMBL10478328;DTXSID00546635;VEPHOUHKTRTFRP-UHFFFAOYSA-N;3,4-dichloro-2-picoline-N-oxide;AKOS006327132;3,4-Dichloro-2-methyl-1-oxo-1lambda~5~-pyridine

Suppliers and Price of 2-Methyl-3,4-dichloropyridine N-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Methyl-3,4-dichloropyridineN-Oxide
250mg
$ 140.00

Medical Isotopes, Inc.
2-Methyl-3,4-dichloropyridineN-Oxide
1.25 g
$ 2000.00

American Custom Chemicals Corporation
2-METHYL-3,4-DICHLOROPYRIDINE-N-OXIDE 95.00%
5MG
$ 504.02

Total 1 raw suppliers

Chemical Property of 2-Methyl-3,4-dichloropyridine N-oxide

Chemical Property:

PSA：25.46000
LogP:2.73030
Solubility.:Chloroform, Dimethyl Sulfoxide, Ethanol
XLogP3:1.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:176.9748192
Heavy Atom Count:10
Complexity:122

Purity/Quality:: 2-Methyl-3,4-dichloropyridineN-Oxide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=[N+](C=CC(=C1Cl)Cl)[O-]
Uses 2-Methyl-3,4-dichloropyridine N-Oxide (cas# 108004-98-4) is a compound useful in organic synthesis.

Technology Process of 2-Methyl-3,4-dichloropyridine N-oxide

There total 4 articles about 2-Methyl-3,4-dichloropyridine N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 3-Chloro-2-methyl-4-nitropyridin-1-oxide

: 108004-98-4
3,4-dichloro-2-methylpyridine N-oxide

Guidance literature:: With hydrogenchloride; Irradiation;

Reference yield:

: 103949-58-2
3,4-dichloro-2-methyl-pyridine

: 108004-98-4
3,4-dichloro-2-methylpyridine N-oxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 - 25 ℃; for 16h;
DOI:10.1021/jm00128a046

Reference yield:

: 18437-58-6
3-methyl-4-pyridinamine

: 108004-98-4
3,4-dichloro-2-methylpyridine N-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / Cl₂, H₂SO₄ / 2 h / 0 °C

2: 96 percent / NaNO₂, conc. HCl / 1) 0 to 5 deg C, 1 h, 2) 25 deg C, 2 h

3: m-chloroperbenzoic acid / CH₂Cl₂ / 16 h / 20 - 25 °C

With hydrogenchloride; sulfuric acid; chlorine; 3-chloro-benzenecarboperoxoic acid; sodium nitrite; In dichloromethane;
DOI:10.1021/jm00128a046