Butanedioic acid, 2-cyano-3-methyl-, 4-ethyl 1-(2-propenyl) ester, (3S)- (9CI)

Base Information

Chemical Name:Butanedioic acid, 2-cyano-3-methyl-, 4-ethyl 1-(2-propenyl) ester, (3S)- (9CI)
CAS No.:454685-94-0
Molecular Formula:C₁₁H₁₅NO₄
Molecular Weight:225.244
Hs Code.:
Mol file:454685-94-0.mol

Synonyms:Butanedioic acid, 2-cyano-3-methyl-, 4-ethyl 1-(2-propenyl) ester, (3S)- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Butanedioic acid, 2-cyano-3-methyl-, 4-ethyl 1-(2-propenyl) ester, (3S)- (9CI)

Chemical Property:

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Technology Process of Butanedioic acid, 2-cyano-3-methyl-, 4-ethyl 1-(2-propenyl) ester, (3S)- (9CI)

There total 2 articles about Butanedioic acid, 2-cyano-3-methyl-, 4-ethyl 1-(2-propenyl) ester, (3S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13361-32-5
allyl cyanoacetate

: 63696-99-1
(S)-ethyl 2-(methylsulfonyloxy)propanoate

: 454685-94-0,154023-28-6,167778-99-6,473445-13-5
(S)-1-Allyl 4-ethyl 2-cyano-3-methylbutanedioate

: 454685-94-0,154023-28-6,167778-99-6,473445-13-5
(R)-1-Allyl 4-ethyl 2-cyano-3-methylbutanedioate

Guidance literature:: With cesium fluoride; In N,N-dimethyl-formamide; Yield given. Yields of byproduct given. Title compound not separated from byproducts; 1.) 1 h, 2.) 45 deg C, 6 h;
DOI:10.1021/jo00113a052

Reference yield:

: 13361-32-5
allyl cyanoacetate

: 63696-99-1
(S)-ethyl 2-(methylsulfonyloxy)propanoate

: 454685-94-0,154023-28-6,167778-99-6,473445-13-5
(S)-1-Allyl 4-ethyl 2-cyano-3-methylbutanedioate

: 454685-94-0,154023-28-6,167778-99-6,473445-13-5
(R)-1-Allyl 4-ethyl 2-cyano-3-methylbutanedioate

Guidance literature:: With cesium fluoride; In N,N-dimethyl-formamide; Yield given. Yields of byproduct given. Title compound not separated from byproducts; 1.) 1 h, 2.) 45 deg C, 6 h;
DOI:10.1021/jo00113a052