benzyl (2-hydroxynaphthalen-1-yl)(2-nitrophenyl)methylcarbamate

Base Information

Chemical Name:benzyl (2-hydroxynaphthalen-1-yl)(2-nitrophenyl)methylcarbamate
CAS No.:1341169-23-0
Molecular Formula:C₂₅H₂₀N₂O₅
Molecular Weight:428.444
Hs Code.:
Mol file:1341169-23-0.mol

Synonyms:benzyl (2-hydroxynaphthalen-1-yl)(2-nitrophenyl)methylcarbamate

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Chemical Property of benzyl (2-hydroxynaphthalen-1-yl)(2-nitrophenyl)methylcarbamate

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Technology Process of benzyl (2-hydroxynaphthalen-1-yl)(2-nitrophenyl)methylcarbamate

There total 1 articles about benzyl (2-hydroxynaphthalen-1-yl)(2-nitrophenyl)methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 621-84-1
O-benzyl carbamate

: 135-19-3
β-naphthol

: 552-89-6
2-nitro-benzaldehyde

: 1341169-23-0
benzyl ((2-nitrophenyl)(2-hydroxynaphthalen-1-yl)methyl) carbamate

Guidance literature:: With graphene oxide supported imidazolium based dicationic ionic liquid; at 80 ℃; for 0.116667h;
DOI:10.1007/s11164-019-03922-0

Reference yield: 69.0%

: 1341169-23-0
benzyl ((2-nitrophenyl)(2-hydroxynaphthalen-1-yl)methyl) carbamate

: 1341169-22-9
1-(amino(2-aminophenyl)methyl)-2-naphthol

Guidance literature:: With palladium on activated charcoal; hydrogen; In methanol; for 2h; under 760.051 Torr;
DOI:10.1016/j.tet.2011.08.074

Reference yield:

: 1341169-23-0
benzyl ((2-nitrophenyl)(2-hydroxynaphthalen-1-yl)methyl) carbamate

: (8RS,15bSR)-phenyl-10,11-dihydro-8H,15bH-naphth[1,2-e][1,3]oxazino[3,4-c]quinazolin-10-one

Guidance literature:: Multi-step reaction with 3 steps

1: palladium on activated charcoal; hydrogen / methanol / 2 h / 760.05 Torr

2: methanol / 24 h / 20 °C

3: sodium carbonate / toluene / 6.5 h / 20 °C / Bomb tube

With palladium on activated charcoal; hydrogen; sodium carbonate; In methanol; toluene;
DOI:10.1016/j.tet.2011.08.074