1(2H)-Pyridineacetic acid, 3-hydroxy-4-methyl-2-oxo-, ethyl ester (9CI)

Base Information

Chemical Name:1(2H)-Pyridineacetic acid, 3-hydroxy-4-methyl-2-oxo-, ethyl ester (9CI)
CAS No.:208592-17-0
Molecular Formula:C₁₀H₁₃NO₄
Molecular Weight:211.218
Hs Code.:
Mol file:208592-17-0.mol

Synonyms:1(2H)-Pyridineacetic acid, 3-hydroxy-4-methyl-2-oxo-, ethyl ester (9CI)

Suppliers and Price of 1(2H)-Pyridineacetic acid, 3-hydroxy-4-methyl-2-oxo-, ethyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1(2H)-Pyridineacetic acid, 3-hydroxy-4-methyl-2-oxo-, ethyl ester (9CI)

Chemical Property:

PSA：68.53000
LogP:0.42540

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1(2H)-Pyridineacetic acid, 3-hydroxy-4-methyl-2-oxo-, ethyl ester (9CI)

There total 3 articles about 1(2H)-Pyridineacetic acid, 3-hydroxy-4-methyl-2-oxo-, ethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 208592-16-9
(3-Hydroxy-4-morpholin-4-ylmethyl-2-oxo-2H-pyridin-1-yl)-acetic acid ethyl ester

: 208592-17-0
N-[(ethoxycarbonyl)methyl]-3-hydroxy-4-methyl-2-(1H)-pyridone

Guidance literature:: palladium on activated charcoal; In ethanol; cyclohexane; for 24h; Heating;
DOI:10.1080/00397919808006860

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 95215-70-6
1-ethoxycarbonylmethyl-3-hydroxy pyrid-2-one

: 208592-17-0
N-[(ethoxycarbonyl)methyl]-3-hydroxy-4-methyl-2-(1H)-pyridone

Guidance literature:: formaldehyd; 1-ethoxycarbonylmethyl-3-hydroxy pyrid-2-one; With morpholine; In ethanol; Inert atmosphere;

With palladium 10% on activated carbon; cyclohexene; regioselective reaction;
DOI:10.1021/ic1009785

Reference yield:

: 95215-70-6
1-ethoxycarbonylmethyl-3-hydroxy pyrid-2-one

: 208592-17-0
N-[(ethoxycarbonyl)methyl]-3-hydroxy-4-methyl-2-(1H)-pyridone

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / ethanol; H₂O / 2 h / Ambient temperature

2: 73 percent / Pd/C / cyclohexane; ethanol / 24 h / Heating

palladium on activated charcoal; In ethanol; cyclohexane; water;
DOI:10.1080/00397919808006860