DI-(4-CARBOXYBENZYL)HYPONITRITE

Base Information

Chemical Name:DI-(4-CARBOXYBENZYL)HYPONITRITE
CAS No.:223507-96-8
Molecular Formula:C16H14NO5-
Molecular Weight:330.297
Hs Code.:
Mol file:223507-96-8.mol

Synonyms:DI-(4-CARBOXYBENZYL)HYPONITRITE;SOTS-1;SUPEROXIDE THERMAL SOURCE;SOTS-1 (technical grade)

Suppliers and Price of DI-(4-CARBOXYBENZYL)HYPONITRITE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Cayman Chemical
SOTS-1 (technical grade) ≥80%
10mg
$ 250.00

Cayman Chemical
SOTS-1 (technical grade) ≥80%
5mg
$ 150.00

Cayman Chemical
SOTS-1 (technical grade) ≥80%
1mg
$ 35.00

Cayman Chemical
SOTS-1 (technical grade) ≥80%
500μg
$ 25.00

AK Scientific
4,4'-[Azobis(oxymethylene)]bis-benzoicacid
5mg
$ 302.00

Total 3 raw suppliers

Chemical Property of DI-(4-CARBOXYBENZYL)HYPONITRITE

Chemical Property:

Boiling Point:548.8±60.0 °C(Predicted)
PKA:3.77±0.10(Predicted)
PSA：117.78000
Density:1.34±0.1 g/cm3(Predicted)
LogP:3.09860

Purity/Quality:

97% ^*data from raw suppliers

SOTS-1 (technical grade) ≥80% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of DI-(4-CARBOXYBENZYL)HYPONITRITE

There total 6 articles about DI-(4-CARBOXYBENZYL)HYPONITRITE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 198834-44-5
bis(4-benzylcarboxybenzyl)hyponitrite

: 223507-96-8
bis(4-carboxybenzyl)hyponitrite

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; methanol; at 0 - 20 ℃; for 4h;
DOI:10.1021/ja993570b

Reference yield: 89.0%

: 291765-74-7
di(4-tert-butylcarboxybenzyl)hyponitrite

: 223507-96-8
bis(4-carboxybenzyl)hyponitrite

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 24h;
DOI:10.1021/ja993570b

Reference yield:

: 52780-16-2
4-bromomethylbenzoyl chloride

: 223507-96-8
bis(4-carboxybenzyl)hyponitrite

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / NaHCO₃ / diethyl ether / 2 h / 20 °C

2: 49 percent / silver hyponitrite / CH₂Cl₂; diethyl ether / 1 h / 0 °C

3: 89 percent / trifluoroacetic acid / CH₂Cl₂ / 24 h / 0 °C

With silver-hydroxylamine; sodium hydrogencarbonate; trifluoroacetic acid; In diethyl ether; dichloromethane; 1: Esterification / 2: Condensation / 3: Elimination;
DOI:10.1021/ja993570b