4-Bromo-2-phenyloxazole

Base Information

Chemical Name:4-Bromo-2-phenyloxazole
CAS No.:861440-59-7
Molecular Formula:C9H6BrNO
Molecular Weight:224.057
Hs Code.:2934999090
European Community (EC) Number:867-001-3
DSSTox Substance ID:DTXSID30479785
Mol file:861440-59-7.mol

Synonyms:4-Bromo-2-phenyloxazole;861440-59-7;4-bromo-2-phenyl-1,3-oxazole;4-BroMo-2-phenyl-oxazole;MFCD12828098;SCHEMBL19378458;DTXSID30479785;AMY30881;AKOS016011696;DS-7016;AC-33813;SY109039;CS-0156384;FT-0737979;EN300-134875;A863295;J-514688

Suppliers and Price of 4-Bromo-2-phenyloxazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynChem
4-BROMO-2-PHENYLOXAZOLE 95%
1 g
$ 850.00

Crysdot
4-Bromo-2-phenyloxazole 97%
1g
$ 720.00

Crysdot
4-Bromo-2-phenyloxazole 97%
250mg
$ 350.00

American Custom Chemicals Corporation
4-BROMO-2-PHENYLOXAZOLE 95.00%
5MG
$ 499.75

AK Scientific
4-Bromo-2-phenyloxazole
1g
$ 709.00

Total 19 raw suppliers

Chemical Property of 4-Bromo-2-phenyloxazole

Chemical Property:

PSA：26.03000
LogP:3.10410
Storage Temp.:under inert gas (nitrogen or Argon) at 2-8°C
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:222.96328
Heavy Atom Count:12
Complexity:148

Purity/Quality:

99%, ^*data from raw suppliers

4-BROMO-2-PHENYLOXAZOLE 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=NC(=CO2)Br

Technology Process of 4-Bromo-2-phenyloxazole

There total 2 articles about 4-Bromo-2-phenyloxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 92629-11-3
5-bromo-2-phenyl-1,3-oxazole

: 861440-59-7
4-bromo-2-phenyloxazole

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 2h; Schlenk technique; Inert atmosphere;
DOI:10.1246/bcsj.20190255

Reference yield:

: 7127-19-7
2-phenyl-1,3-oxazoline

: 861440-59-7
4-bromo-2-phenyloxazole

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / Inert atmosphere; Schlenk technique; Reflux

2: lithium diisopropyl amide / tetrahydrofuran / 2 h / -78 °C / Schlenk technique; Inert atmosphere

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); lithium diisopropyl amide; In tetrahydrofuran; tetrachloromethane;
DOI:10.1246/bcsj.20190255

Reference yield: 97.0%

: 861440-59-7
4-bromo-2-phenyloxazole

: 74-88-4
methyl iodide

: 197719-26-9
4-bromo-5-methyl-2-phenyloxazole

Guidance literature:: 4-bromo-2-phenyloxazole; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃;

methyl iodide; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1039/c2cc35587f