Diethyl (10-aminodecyl)phosphonate

Base Information

Chemical Name:Diethyl (10-aminodecyl)phosphonate
CAS No.:120818-69-1
Molecular Formula:C₁₄H₃₂NO₃P
Molecular Weight:293.387
Hs Code.:
DSSTox Substance ID:DTXSID501237566
Mol file:120818-69-1.mol

Synonyms:Diethyl (10-aminodecyl)phosphonate;120818-69-1;10-diethoxyphosphoryldecan-1-amine;SCHEMBL15927961;Diethyl(10-aminodecyl)phosphonate;DTXSID501237566;MFCD16876760;AKOS017343406;Phosphonic acid, (10-aminodecyl)-, diethyl ester

Suppliers and Price of Diethyl (10-aminodecyl)phosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of Diethyl (10-aminodecyl)phosphonate

Chemical Property:

PSA：71.36000
LogP:5.03230
XLogP3:2.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:14
Exact Mass:293.21198088
Heavy Atom Count:19
Complexity:227

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOP(=O)(CCCCCCCCCCN)OCC

Technology Process of Diethyl (10-aminodecyl)phosphonate

There total 3 articles about Diethyl (10-aminodecyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 120818-68-0
[10-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-decyl]-phosphonic acid diethyl ester

: 120818-69-1
(10-Amino-decyl)-phosphonic acid diethyl ester

Guidance literature:: [10-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-decyl]-phosphonic acid diethyl ester; With hydrazine; In ethanol; water; at 0 ℃; for 0.5h;

for 10h; Reflux;
DOI:10.3390/molecules26040877

Reference yield:

: 24566-80-1
N-(10-bromodecyl)phthalimide

: 120818-69-1
(10-Amino-decyl)-phosphonic acid diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / 16 h / 140 °C

2: 79 percent / NH₂NH₂, triethylamine / ethanol

With triethylamine; hydrazine; In ethanol;
DOI:10.1016/S0040-4039(00)80807-2

Reference yield:

: 4101-68-2
1,10-dibromodecane

: 120818-69-1
(10-Amino-decyl)-phosphonic acid diethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: N,N-dimethyl-formamide / 7 h / 160 °C

2.1: 24 h / 150 °C

3.1: hydrazine / water; ethanol / 0.5 h / 0 °C

3.2: 10 h / Reflux

With hydrazine; In ethanol; water; N,N-dimethyl-formamide; 2.1: |Michaelis-Arbuzov Synthesis / 3.1: |Gabriel Amine Synthesis;
DOI:10.3390/molecules26040877