Benzyl 2-O,3-O-isopropylidene-α-D-mannofuranoside bis(methanesulfonate)

Base Information

• Chemical Name: Benzyl 2-O,3-O-isopropylidene-α-D-mannofuranoside bis(methanesulfonate)
• CAS No.: 28978-37-2
• Molecular Formula: C18H26O10S2
• Molecular Weight: 466.53
• Mol file: 28978-37-2.mol

Synonyms:Benzyl 2-O,3-O-isopropylidene-α-D-mannofuranoside bis(methanesulfonate)

Chemical Property of Benzyl 2-O,3-O-isopropylidene-α-D-mannofuranoside bis(methanesulfonate)

Chemical Property:

• Melting Point: 107 - 109 °C
• PSA: 140.42000
• LogP: 2.93080

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzyl 2-O,3-O-isopropylidene-α-D-mannofuranoside bis(methanesulfonate)

There total 3 articles about Benzyl 2-O,3-O-isopropylidene-α-D-mannofuranoside bis(methanesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1-O-benzyl-2,3-O-isopropylidene-α-D-manno-furanose (74912-02-0,79940-48-0,94118-99-7,20689-03-6) + methanesulfonyl chloride (124-63-0) → 1-O-benzyl-2,3-O-isopropylidene-5,6-di-O-mesyl-α-D-mannofuranose (28978-37-2)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1002/adsc.201600903

Reference yield:

→ 1-O-benzyl-2,3-O-isopropylidene-5,6-di-O-mesyl-α-D-mannofuranose (28978-37-2)

Guidance literature:

(5), CH3SO2Cl;

DOI:10.1016/S0008-6215(00)80603-5

Reference yield:

→ Benzyl-2,3-isopropyliden-5,6-bis-O-methylsulfonyl-α-D-mannofuranosid (28978-37-2)

Guidance literature:

Benzyl-2,3-isopropyliden-α-D-mannofuranosid, Methansulfonylchlorid/Py.;

upstream raw materials:

1-O-benzyl-2,3-O-isopropylidene-α-D-manno-furanose

methanesulfonyl chloride

Downstream raw materials:

5,6-di-O-acetyl-1-O-benzyl-2,3-O-isopropylidene-β-L-gulofuranose

phenylmethyl-2,3-O-(1-methylethylidene)-5,6-didehydro-5,6-dideoxy-α-D-mannofuranoside

1-deoxymannojirimycin

benzyl 5-azido-5-deoxy-α-D-mannofuranoside

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