2,3-DIHYDRO-1-(IODOMETHYL)-1H-INDENE

Base Information

Chemical Name:2,3-DIHYDRO-1-(IODOMETHYL)-1H-INDENE
CAS No.:107657-96-5
Molecular Formula:C10H11I
Molecular Weight:258.102
Hs Code.:
Mol file:107657-96-5.mol

Synonyms:2,3-DIHYDRO-1-(IODOMETHYL)-1H-INDENE

Suppliers and Price of 2,3-DIHYDRO-1-(IODOMETHYL)-1H-INDENE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2,3-DIHYDRO-1-(IODOMETHYL)-1H-INDENE

Chemical Property:

PSA：0.00000
LogP:3.15140

Purity/Quality:: 98%Min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,3-DIHYDRO-1-(IODOMETHYL)-1H-INDENE

There total 4 articles about 2,3-DIHYDRO-1-(IODOMETHYL)-1H-INDENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 107616-48-8
2-(but-3-en-1-yl)benzenediazonium hexafluorophosphate

: 24892-64-6
1-(but-3-en-1-yl)-2-iodobenzene

: 107657-96-5
1-(iodomethyl)indane

Guidance literature:: With sodium iodide; In acetone; for 0.25h; Yield given;
DOI:10.1021/jo00386a007

Reference yield:

: 24892-64-6
1-(but-3-en-1-yl)-2-iodobenzene

: 768-56-9
4-Phenylbut-1-ene

: 767-60-2
3-Methylindene

: 107657-96-5
1-(iodomethyl)indane

Guidance literature:: With tert-butyl methyl ether; N,N,N,N,-tetramethylethylenediamine; phenyllithium; In diethyl ether; cyclohexane; pentane; at 60 ℃; for 7h;
DOI:10.1021/jo981991q

Reference yield:

: 6992-97-8
2-(but-3-en-1-yl)aniline

: 107657-96-5
1-(iodomethyl)indane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaNO₂, conc. HCl, 2.) HPF₆ / 1.) H₂O, 0 deg C

2: 66 percent / NaI / acetone / 0.25 h

With hydrogenchloride; hexafluorophosphoric acid; sodium iodide; sodium nitrite; In acetone;
DOI:10.1021/jo00386a007