2-(but-3-en-1-yl)benzenediazonium hexafluorophosphate

Base Information

Chemical Name:2-(but-3-en-1-yl)benzenediazonium hexafluorophosphate
CAS No.:107616-48-8
Molecular Formula:C₁₀H₁₁N₂*F₆P
Molecular Weight:304.175
Hs Code.:

Synonyms:2-(but-3-en-1-yl)benzenediazonium hexafluorophosphate

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Chemical Property of 2-(but-3-en-1-yl)benzenediazonium hexafluorophosphate

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Technology Process of 2-(but-3-en-1-yl)benzenediazonium hexafluorophosphate

There total 6 articles about 2-(but-3-en-1-yl)benzenediazonium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 6992-97-8
2-(but-3-en-1-yl)aniline

: 107616-48-8
2-(but-3-en-1-yl)benzenediazonium hexafluorophosphate

Guidance literature:: 2-(but-3-en-1-yl)aniline; With hydrogenchloride; sodium nitrite; In water; at 0 ℃; for 0.666667h; Inert atmosphere;

With hexafluorophosphoric acid; In water; for 0.166667h; Inert atmosphere;
DOI:10.1002/anie.201802466

Reference yield:

: 274676-13-0
methyl (+/-)-2-(2-nitrophenyl)-4-pentenoate

: 107616-48-8
2-(but-3-en-1-yl)benzenediazonium hexafluorophosphate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / 1,4-dioxane / 3 h / 20 °C / Reflux; Inert atmosphere

1.2: 0.75 h / 50 °C / Inert atmosphere

2.1: acetic acid; zinc / 12 h / 20 °C / Inert atmosphere

3.1: sodium nitrite; hydrogenchloride / water / 0.67 h / 0 °C / Inert atmosphere

3.2: 0.17 h / Inert atmosphere

With hydrogenchloride; acetic acid; sodium hydroxide; zinc; sodium nitrite; In 1,4-dioxane; water;
DOI:10.1002/anie.201802466

Reference yield:

: 3740-52-1
2-(2-nitrophenyl)acetic acid

: 107616-48-8
2-(but-3-en-1-yl)benzenediazonium hexafluorophosphate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid / 4 h / Reflux; Inert atmosphere

2.1: potassium carbonate; 18-crown-6 ether / methanol / 8 h / Reflux; Inert atmosphere

3.1: sodium hydroxide / 1,4-dioxane / 3 h / 20 °C / Reflux; Inert atmosphere

3.2: 0.75 h / 50 °C / Inert atmosphere

4.1: acetic acid; zinc / 12 h / 20 °C / Inert atmosphere

5.1: sodium nitrite; hydrogenchloride / water / 0.67 h / 0 °C / Inert atmosphere

5.2: 0.17 h / Inert atmosphere

With hydrogenchloride; 18-crown-6 ether; sulfuric acid; potassium carbonate; acetic acid; sodium hydroxide; zinc; sodium nitrite; In 1,4-dioxane; methanol; water;
DOI:10.1002/anie.201802466