1H-1,4-Diazepine,1-ethylhexahydro-4-(1-methylethyl)-6-nitro-(9CI)

Base Information

Chemical Name:1H-1,4-Diazepine,1-ethylhexahydro-4-(1-methylethyl)-6-nitro-(9CI)
CAS No.:483303-69-1
Molecular Formula:C₁₀H₂₁N₃O₂
Molecular Weight:215.296
Hs Code.:
Mol file:483303-69-1.mol

Synonyms:1H-1,4-Diazepine,1-ethylhexahydro-4-(1-methylethyl)-6-nitro-(9CI)

Suppliers and Price of 1H-1,4-Diazepine,1-ethylhexahydro-4-(1-methylethyl)-6-nitro-(9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-1,4-Diazepine,1-ethylhexahydro-4-(1-methylethyl)-6-nitro-(9CI)

Chemical Property:

PSA：0.00000
LogP:0.00000

Purity/Quality:

Safty Information:

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Hazard Codes:

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Technology Process of 1H-1,4-Diazepine,1-ethylhexahydro-4-(1-methylethyl)-6-nitro-(9CI)

There total 4 articles about 1H-1,4-Diazepine,1-ethylhexahydro-4-(1-methylethyl)-6-nitro-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 483303-67-9
1-ethyl-6-hydroxymethyl-4-isopropyl-6-nitrohexahydro-1,4-diazepine

: 483303-69-1
1-ethyl-4-isopropyl-6-nitrohexahydro-1,4-diazepine

Guidance literature:: 1-ethyl-6-hydroxymethyl-4-isopropyl-6-nitrohexahydro-1,4-diazepine; With potassium tert-butylate; In methanol; at 50 ℃; for 0.5h;

With hydroxylamine hydrochloride; In water;
DOI:10.1248/cpb.50.941

Reference yield:

: 109-56-8
i-propyl(2-(hydroxy)ethyl)amine

: 483303-69-1
1-ethyl-4-isopropyl-6-nitrohexahydro-1,4-diazepine

Guidance literature:: Multi-step reaction with 4 steps

1.1: 99 percent / SOCl₂ / CHCl₃ / 6 h / Heating

2.1: 26 percent / ethanol; H₂O / 16 h / 50 °C

3.1: aq. NaHCO₃ / 2 h / 40 - 50 °C

4.1: t-BuOK / methanol / 0.5 h / 50 °C

4.2: 4.3 g / NH₂OH*HCl / H₂O

With thionyl chloride; potassium tert-butylate; sodium hydrogencarbonate; In methanol; ethanol; chloroform; water;
DOI:10.1248/cpb.50.941

Reference yield:

: 32776-20-8
N-ethyl-N'-isopropylethylenediamine

: 483303-69-1
1-ethyl-4-isopropyl-6-nitrohexahydro-1,4-diazepine

Guidance literature:: Multi-step reaction with 2 steps

1.1: aq. NaHCO₃ / 2 h / 40 - 50 °C

2.1: t-BuOK / methanol / 0.5 h / 50 °C

2.2: 4.3 g / NH₂OH*HCl / H₂O

With potassium tert-butylate; sodium hydrogencarbonate; In methanol;
DOI:10.1248/cpb.50.941