Butanoic acid, 4-(dimethylamino)-4-thioxo-, 4-hydroxybutyl ester

Base Information

Chemical Name:Butanoic acid, 4-(dimethylamino)-4-thioxo-, 4-hydroxybutyl ester
CAS No.:73199-73-2
Molecular Formula:C₁₀H₁₉NO₃S
Molecular Weight:233.332
Hs Code.:
Mol file:73199-73-2.mol

Synonyms:Butanoic acid, 4-(dimethylamino)-4-thioxo-, 4-hydroxybutyl ester

Suppliers and Price of Butanoic acid, 4-(dimethylamino)-4-thioxo-, 4-hydroxybutyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of Butanoic acid, 4-(dimethylamino)-4-thioxo-, 4-hydroxybutyl ester

Chemical Property:

PSA：81.86000
LogP:0.97130

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Butanoic acid, 4-(dimethylamino)-4-thioxo-, 4-hydroxybutyl ester

There total 2 articles about Butanoic acid, 4-(dimethylamino)-4-thioxo-, 4-hydroxybutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 110-63-4
Butane-1,4-diol

: 73199-96-9
Methyl 3-(Dimethylthiocarbamoyl)propanoate

: 73199-73-2
4-Hydroxybutyl-3-(dimethylthiocarbamoyl)propanoate

Guidance literature:: With sodium methylate; for 1h; pressure < 1 mm;
DOI:10.1021/jo01298a022

Reference yield:

: 30891-34-0
methyl 3-(dimethylcarbamoyl)-propanoate

: 73199-73-2
4-Hydroxybutyl-3-(dimethylthiocarbamoyl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / phosphorus pentasulfide, triethylamine / CH₂Cl₂ / 24 h / Heating

2: 61 percent / sodium methoxide / 1 h / pressure < 1 mm

With diphosphorus pentasulfide; sodium methylate; triethylamine; In dichloromethane;
DOI:10.1021/jo01298a022